2,2-Dimethyl-2,3-dihydrobenzoselenophene

Base Information

• Chemical Name: 2,2-Dimethyl-2,3-dihydrobenzoselenophene
• CAS No.: 60096-27-7
• Molecular Formula: C₁₀H₁₂Se
• Molecular Weight: 211.165
• DSSTox Substance ID: DTXSID10208838
• Nikkaji Number: J1.920.121J
• Wikidata: Q83082997

Synonyms:2,2-Dimethyl-2,3-dihydrobenzoselenophene;60096-27-7;DTXSID10208838

Chemical Property of 2,2-Dimethyl-2,3-dihydrobenzoselenophene

Chemical Property:

• Vapor Pressure: 0.0313mmHg at 25°C
• Boiling Point: 252.2°C at 760 mmHg
• Flash Point: 106.3°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 212.01042
• Heavy Atom Count: 11
• Complexity: 151

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CC2=CC=CC=C2[Se]1)C

Technology Process of 2,2-Dimethyl-2,3-dihydrobenzoselenophene

There total 2 articles about 2,2-Dimethyl-2,3-dihydrobenzoselenophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

2-methyl-3-prop-2-enyl phenylselenide (59085-70-0) → 2,2-dimethyl-2,3-dihydrobenzo[b]selenophene (60096-27-7)

Guidance literature:

In quinoline; at 210 ℃; for 2h;

DOI:10.1081/SCC-120021044

Reference yield:

→ 2,2-dimethyl-2,3-dihydrobenzo[b]selenophene (60096-27-7)

Guidance literature:

Erhitzen von CH2=C(CH3)-CH2-Se-Ph mit Chinolin;

DOI:10.1021/jo00403a016

Reference yield:

2,2-dimethyl-2,3-dihydrobenzo[b]selenophene (60096-27-7) + methyl iodide (74-88-4) → (o-Methallyl-phenyl)-methylselenid (60430-47-9)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00403a016

upstream raw materials:

2-methyl-3-prop-2-enyl phenylselenide

Downstream raw materials:

(o-Methallyl-phenyl)-methylselenid

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