1,2,4-Methenopentalene-5-carboxaldehyde, octahydro-, [1R-(1alpha,2alpha,3abeta,4alpha,5beta,6abeta,7S*)]- (9CI)

Base Information

Chemical Name:1,2,4-Methenopentalene-5-carboxaldehyde, octahydro-, [1R-(1alpha,2alpha,3abeta,4alpha,5beta,6abeta,7S*)]- (9CI)
CAS No.:144940-34-1
Molecular Formula:C₁₀H₁₂O
Molecular Weight:148.205
Hs Code.:
Mol file:144940-34-1.mol

Synonyms:1,2,4-Methenopentalene-5-carboxaldehyde, octahydro-, [1R-(1alpha,2alpha,3abeta,4alpha,5beta,6abeta,7S*)]- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,4-Methenopentalene-5-carboxaldehyde, octahydro-, [1R-(1alpha,2alpha,3abeta,4alpha,5beta,6abeta,7S*)]- (9CI)

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Technology Process of 1,2,4-Methenopentalene-5-carboxaldehyde, octahydro-, [1R-(1alpha,2alpha,3abeta,4alpha,5beta,6abeta,7S*)]- (9CI)

There total 4 articles about 1,2,4-Methenopentalene-5-carboxaldehyde, octahydro-, [1R-(1alpha,2alpha,3abeta,4alpha,5beta,6abeta,7S*)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 201230-82-2
carbon monoxide

: 7785-10-6
deltacyclene

: 6567-11-9
deltacyclane

: 144917-49-7,144940-34-1,144940-35-2,171965-33-6,171965-34-7
C₁₀H₁₂O

: 144917-49-7,144940-34-1,144940-35-2,171965-33-6,171965-34-7
4-exo-formyl-deltacyclane

Guidance literature:: With hydrogen; tin(ll) chloride; PtCl2<(R)-PROPHOS>; In toluene; at 100 ℃; for 10h; under 30002.4 Torr;
DOI:10.1016/S0957-4166(00)86031-0

Reference yield: 93.0%

: 201230-82-2
carbon monoxide

: 7785-10-6
deltacyclene

: 6567-11-9
deltacyclane

: 144917-49-7,144940-34-1,144940-35-2,171965-33-6,171965-34-7
C₁₀H₁₂O

: 144917-49-7,144940-34-1,144940-35-2,171965-33-6,171965-34-7
4-exo-formyl-deltacyclane

Guidance literature:: With hydrogen; tin(ll) chloride; PtCl2<(R)-PROPHOS>; In toluene; at 100 ℃; for 10h; under 30002.4 Torr;
DOI:10.1016/S0957-4166(00)86031-0

Reference yield: 93.0%

: 201230-82-2
carbon monoxide

: 7785-10-6
deltacyclene

: 144917-49-7,144940-34-1,144940-35-2,171965-33-6,171965-34-7
C₁₀H₁₂O

: 144917-49-7,144940-34-1,144940-35-2,171965-33-6,171965-34-7
4-exo-formyl-deltacyclane

Guidance literature:: [Rh(norbornadiene)Cl]2; triphenylphosphine; In toluene; at 100 ℃; for 8h; under 30002.4 Torr; Product distribution; var. temp. and time, var. optically active rhodium-phosphine and platinium-phosphine-tin(II)chloride catalysts;
DOI:10.1016/S0957-4166(00)86031-0