N-(Tert-butoxycarbonyl)glycine-2-13C-15N

Base Information

Chemical Name:N-(Tert-butoxycarbonyl)glycine-2-13C-15N
CAS No.:145143-01-7
Molecular Formula:C7H13 N O4
Molecular Weight:177.2
Hs Code.:
European Community (EC) Number:693-253-7
DSSTox Substance ID:DTXSID10583955
Wikidata:Q82475573
Mol file:145143-01-7.mol

Synonyms:145143-01-7;N-(TERT-BUTOXYCARBONYL)GLYCINE-2-13C-15N;2-[(2-Methylpropan-2-yl)oxycarbonyl(15N)amino]acetic acid;Boc-Gly-OH-2-13C,15N;starbld0016648;N-(tert-Butoxycarbonyl)(2-~13~C,~15~N)glycine;DTXSID10583955;Boc-Gly-OH-2-13C,15N, 98 atom % 15N, 99 atom % 13C

Suppliers and Price of N-(Tert-butoxycarbonyl)glycine-2-13C-15N

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Boc-Gly-OH-2-13C,15N 98 atom %
100mg
$ 880.00

American Custom Chemicals Corporation
BOC-GLY-OH-2-13C,15N 95.00%
100MG
$ 1223.67

Total 2 raw suppliers

Chemical Property of N-(Tert-butoxycarbonyl)glycine-2-13C-15N

Chemical Property:

Melting Point:86-89 °C(lit.)
PSA：75.63000
LogP:0.98660
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:177.08484763
Heavy Atom Count:12
Complexity:182

Purity/Quality:

98% by CP; 99% atom 13C; 98% atom 15N ^*data from raw suppliers

Boc-Gly-OH-2-13C,15N 98 atom % ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22-41
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCC(=O)O
Isomeric SMILES:CC(C)(C)OC(=O)[15NH][13CH2]C(=O)O

Technology Process of N-(Tert-butoxycarbonyl)glycine-2-13C-15N

There total 2 articles about N-(Tert-butoxycarbonyl)glycine-2-13C-15N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 145142-96-7
C₈⁽¹³⁾CH₁₇⁽¹⁵⁾NO₄

: 145143-01-7
[13Cα,15N]-N-BOC-glycine

Guidance literature:: saponification;
DOI:10.1039/c39920001332

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 91795-59-4
<2-¹³C, ¹⁵N>glycine

: 145143-01-7
[13Cα,15N]-N-BOC-glycine

Guidance literature:: With sodium hydroxide; In tert-butyl alcohol;
DOI:10.1021/ja026700g

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 145143-01-7
[13Cα,15N]-N-BOC-glycine

: C₁₂⁽¹³⁾CH₁₇N₂⁽¹⁵⁾NO₄

Guidance literature:: [13Cα,15N]-N-BOC-glycine; glycine resin; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; In N,N-dimethyl-formamide; solid state reaction;

N-tert-butoxycarbonyl-L-phenylalanine;

With hydrogen fluoride; Further stages.;
DOI:10.1021/ja026700g