1-chloro-N-phenylcyclohexanecarboxamide

Base Information

Chemical Name:1-chloro-N-phenylcyclohexanecarboxamide
CAS No.:4664-73-7
Molecular Formula:C13H16 Cl N O
Molecular Weight:237.729
Hs Code.:
Mol file:4664-73-7.mol

Synonyms:Cyclohexanecarboxanilide,1-chloro- (7CI,8CI); NSC 289475

Suppliers and Price of 1-chloro-N-phenylcyclohexanecarboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 1-chloro-N-phenylcyclohexanecarboxamide

Chemical Property:

Vapor Pressure:3.7E-07mmHg at 25°C
Boiling Point:416.9°C at 760 mmHg
Flash Point:205.9°C
Density:1.17g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-chloro-N-phenylcyclohexanecarboxamide

There total 4 articles about 1-chloro-N-phenylcyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1-bromo-N-phenylcyclohexane-1-carboxamide

: 4664-73-7
1-Chlor-cyclohexan-1-carbonsaeure-anilid

Guidance literature:: With hexaaquocopper(II) tetrafluoroborate; dichloromethane; N,N,N',N'',N'''-pentamethyldiethylenetriamine; at 100 ℃; for 1h; Inert atmosphere;
DOI:10.1246/cl.170062

Reference yield:

: 2719-26-8
N-phenylcyclohexanamide

: 4664-73-7
1-Chlor-cyclohexan-1-carbonsaeure-anilid

Guidance literature:: Multistep reaction; (i) PCl₅, benzene, (ii) H₂O;
DOI:10.1021/jo01023a002

Reference yield:

: 62-53-3
aniline

: 4664-73-7
1-Chlor-cyclohexan-1-carbonsaeure-anilid

Guidance literature:: Multi-step reaction with 2 steps

1: (i) SOCl₂, (ii) /BRN= 605631/, benzene

2: (i) PCl₅, benzene, (ii) H₂O

DOI:10.1021/jo01023a002