Technology Process of 1,2-DIIODO-4,5-(DIDODECYLOXY)BENZENE
There total 3 articles about 1,2-DIIODO-4,5-(DIDODECYLOXY)BENZENE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodic peroxide; iodine; acetic acid;
sulfuric acid;
In
water;
at 70 ℃;
for 6h;
DOI:10.1021/ja0655441
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / dimethylformamide / 1 h / 20 °C
1.2: 77 percent / dimethylformamide / 6 h / 80 °C
2.1: 95 percent / iodine; iodic peroxide; acetic acid / H2SO4 / H2O / 6 h / 70 °C
With
iodic peroxide; iodine; potassium carbonate; acetic acid;
sulfuric acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1021/ja0655441
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / dimethylformamide / 1 h / 20 °C
1.2: 77 percent / dimethylformamide / 6 h / 80 °C
2.1: 95 percent / iodine; iodic peroxide; acetic acid / H2SO4 / H2O / 6 h / 70 °C
With
iodic peroxide; iodine; potassium carbonate; acetic acid;
sulfuric acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1021/ja0655441
