1,4-DIDEOXY-1,4-IMINO-D-XYLITOL HYDROCHLORIDE

Base Information

• Chemical Name: 1,4-DIDEOXY-1,4-IMINO-D-XYLITOL HYDROCHLORIDE
• CAS No.: 52019-89-3
• Molecular Formula: C₅H₁₁NO₃
• Molecular Weight: 133.147
• Mol file: 52019-89-3.mol

Synonyms:1,4-DIDEOXY-1,4-IMINO-D-XYLITOL HYDROCHLORIDE;1,4-DIDEOXY-1,4-IMINO-D-XYLITOL

Chemical Property of 1,4-DIDEOXY-1,4-IMINO-D-XYLITOL HYDROCHLORIDE

Chemical Property:

• PSA: 72.72000
• LogP: -1.19690

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-DIDEOXY-1,4-IMINO-D-XYLITOL HYDROCHLORIDE

There total 33 articles about 1,4-DIDEOXY-1,4-IMINO-D-XYLITOL HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2S,3S,4S)-2-benzyloxymethyl-3,4-dibenzyloxy-pyrrolidin (100806-55-1) → (2S,3S,4S)-2-(hydroxymethyl)pyrrolidine-3,4-diol (52019-89-3,97058-12-3,98632-49-6,100937-51-7,100937-52-8,100937-53-9,105990-40-7,105990-41-8,105990-42-9,129568-47-4,186759-56-8,187339-50-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 10h;

DOI:10.1016/j.tet.2007.02.087

Reference yield: 96.0%

Benzoic acid (2S,3S,4R)-3,4-dihydroxy-5-oxo-pyrrolidin-2-ylmethyl ester (186025-81-0) → (2S,3S,4S)-2-(hydroxymethyl)pyrrolidine-3,4-diol (52019-89-3,97058-12-3,98632-49-6,100937-51-7,100937-52-8,100937-53-9,105990-40-7,105990-41-8,105990-42-9,129568-47-4,186759-56-8,187339-50-0)

Guidance literature:

With diborane; In tetrahydrofuran; Heating;

DOI:10.1021/jo962028s

Reference yield: 91.0%

(2S,3S,4S)-2-Hydroxymethyl-1-(4-methoxy-benzyl)-pyrrolidine-3,4-diol (245484-08-6) → (2S,3S,4S)-2-(hydroxymethyl)pyrrolidine-3,4-diol (52019-89-3,97058-12-3,98632-49-6,100937-51-7,100937-52-8,100937-53-9,105990-40-7,105990-41-8,105990-42-9,129568-47-4,186759-56-8,187339-50-0)

Guidance literature:

With formic acid; hydrogen; palladium dihydroxide; In ethanol; for 1h;

DOI:10.1016/S0040-4020(97)00445-6

upstream raw materials:

(2S,3S,4S)-2-benzyloxymethyl-3,4-dibenzyloxy-pyrrolidin

1-azido-1-deoxy-4-O-methanesulphonyl-2,3,5-tri-O-benzyl-D-xylitol

methyl 4-azido-4-deoxy-β-L-arabinopyranoside

(2S,3S,4S)-2-Hydroxymethyl-1-(4-methoxy-benzyl)-pyrrolidine-3,4-diol

Downstream raw materials:

1,4-dideoxy-1,4-imino-L-arabinitol hydrochloride

(2S,3S,4S)-3,4-dihydroxy-2-hydroxymethyl-1-methylpyrrolidine

(2S,3S,4S)-3,4-diacetoxy-2-[(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyloxy)methyl]pyrrolidine

(2S,3S,4S)-3,4-dihydroxy-1-(tert-butoxycarbonyl)-2-[(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyloxy)methyl]pyrrolidine

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