D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-

Base Information

Chemical Name:D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-
CAS No.:149625-44-5
Molecular Formula:C21H33 N O7
Molecular Weight:411.49
Hs Code.:
Mol file:149625-44-5.mol

Synonyms:D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-

Suppliers and Price of D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-

Chemical Property:

PSA：106.48000
LogP:2.36070

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-

There total 8 articles about D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125158-55-6
2-methyl-(3-O-benzyl-1,2-dideoxy-5,6-O-isopropylidene-α-D-glucofurano)-<2.1-d>-2-oxazoline

: 149625-44-5
3-O-benzyl-2-t-butyloxycarbonylamino-2-deoxy-5,6-O-isopropylidene-D-glucitol

Guidance literature:: Multi-step reaction with 5 steps

1: 10percent aq. HOAc / methanol / 7 h / Ambient temperature

2: NaBH₄ / methanol / 1 h / Ambient temperature

3: pyridine / Ambient temperature

4: 1M aq. NaOH / methanol / 7 h / Heating

5: KHCO₃ / dioxane; H₂O / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; potassium hydrogencarbonate; acetic acid; In 1,4-dioxane; pyridine; methanol; water;
DOI:10.1016/S0040-4020(01)89338-8

Reference yield:

: 125158-56-7,125158-58-9
2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-D-glucofuranose

: 149625-44-5
3-O-benzyl-2-t-butyloxycarbonylamino-2-deoxy-5,6-O-isopropylidene-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / methanol / 1 h / Ambient temperature

2: pyridine / Ambient temperature

3: 1M aq. NaOH / methanol / 7 h / Heating

4: KHCO₃ / dioxane; H₂O / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; potassium hydrogencarbonate; In 1,4-dioxane; pyridine; methanol; water;
DOI:10.1016/S0040-4020(01)89338-8

Reference yield:

: 149625-48-9
2-acetamido-3-O-benzyl-2-deoxy-5,6-O-isopropylidene-D-glucitol

: 149625-44-5
3-O-benzyl-2-t-butyloxycarbonylamino-2-deoxy-5,6-O-isopropylidene-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / Ambient temperature

2: 1M aq. NaOH / methanol / 7 h / Heating

3: KHCO₃ / dioxane; H₂O / Ambient temperature

With sodium hydroxide; potassium hydrogencarbonate; In 1,4-dioxane; pyridine; methanol; water;
DOI:10.1016/S0040-4020(01)89338-8