Technology Process of D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-, 1,4-dimethanesulfonate
There total 9 articles about D-Glucitol, 2-deoxy-2-(1,1-dimethylethoxy)carbonylamino-5,6-O-(1-methylethylidene)-3-O-(phenylmethyl)-, 1,4-dimethanesulfonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: KHCO3 / dioxane; H2O / Ambient temperature
2: 82 percent / pyridine
With
potassium hydrogencarbonate;
In
1,4-dioxane; pyridine; water;
DOI:10.1016/S0040-4020(01)89338-8
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 80percent oily NaH / dimethylformamide / Ambient temperature
2: 10percent aq. HOAc / methanol / 7 h / Ambient temperature
3: NaBH4 / methanol / 1 h / Ambient temperature
4: pyridine / Ambient temperature
5: 1M aq. NaOH / methanol / 7 h / Heating
6: KHCO3 / dioxane; H2O / Ambient temperature
7: 82 percent / pyridine
With
sodium hydroxide; sodium tetrahydroborate; sodium hydride; potassium hydrogencarbonate; acetic acid;
In
1,4-dioxane; pyridine; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89338-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: KHCO3 / dioxane; H2O / Ambient temperature
2: 82 percent / pyridine
With
potassium hydrogencarbonate;
In
1,4-dioxane; pyridine; water;
DOI:10.1016/S0040-4020(01)89338-8