Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:149324-85-6
Molecular Formula:C14H20 O3
Molecular Weight:236.311
Hs Code.:
Mol file:149324-85-6.mol

Synonyms:Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

PSA：46.53000
LogP:3.08530

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)

There total 4 articles about Benzoic acid, 4-(1-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65874-27-3
4-(tert-butoxycarbonyl)benzaldehyde

: 149324-85-6
4-(t-butoxycarbonyl)phenylpropanol

Guidance literature:: ethylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; diethyl ether; at -23 ℃; for 0.333333h;

4-(tert-butoxycarbonyl)benzaldehyde; In tetrahydrofuran; diethyl ether; at -23 ℃; for 0.5h;

With ammonia; ammonium chloride; In tetrahydrofuran; diethyl ether; water; at 20 ℃; for 0.666667h;

Reference yield:

: 925-90-6
ethylmagnesium bromide

: 65874-27-3
4-(tert-butoxycarbonyl)benzaldehyde

: 149324-85-6
4-(t-butoxycarbonyl)phenylpropanol

Guidance literature:: With copper(l) iodide; In diethyl ether; at -23 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2007.03.085

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 149324-85-6
4-(t-butoxycarbonyl)phenylpropanol

Guidance literature:: Multi-step reaction with 2 steps

1: 2-methyl-propan-2-ol; CH₂Cl₂ / 16 h / 20 °C

2: CuI / diethyl ether / 0.5 h / -23 °C

With copper(l) iodide; In diethyl ether; dichloromethane; tert-butyl alcohol; 2: Grignard reaction;
DOI:10.1016/j.bmcl.2007.03.085