Butane(dithioic) acid, 3-oxo- (9CI)

Base Information

• Chemical Name: Butane(dithioic) acid, 3-oxo- (9CI)
• CAS No.: 151323-87-4
• Molecular Formula: C₄H₆OS₂
• Molecular Weight: 134.223
• Mol file: 151323-87-4.mol

Synonyms:Butane(dithioic) acid, 3-oxo- (9CI)

Chemical Property of Butane(dithioic) acid, 3-oxo- (9CI)

Chemical Property:

• PSA: 87.96000
• LogP: 1.22270

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Butane(dithioic) acid, 3-oxo- (9CI)

There total 1 articles about Butane(dithioic) acid, 3-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + acetone (67-64-1) → 3-Oxo-dithiobutansaeure (151323-87-4)

Guidance literature:

With methanesulfonic acid; potassium tert-butylate; Multistep reaction; 1.) THF, 2 h, 2.) ice bath;

DOI:10.1016/S0040-4039(00)79205-7

Reference yield:

3-Oxo-dithiobutansaeure (151323-87-4) → 3,3'-dithiobis(5-methyl-1H-pyrazole) (288155-30-6)

Guidance literature:

With hydrazine hydrate; In ethanol; at 0 - 20 ℃; for 18h; Reflux;

upstream raw materials:

carbon disulfide

acetone

Downstream raw materials:

3,3'-dithiobis(5-methyl-1H-pyrazole)

Refernces

• 1、 -. "ALKYLAMINOPYRIDINE DERIVATIVE". Page/Page column 51; 52. . Retrieved 2011/01/11.
• 2、 Curphey, Thomas J.,Joyner, H. Howard. "Synthesis of 3H-1,2-dithiole-3-thiones by a novel oxidative cyclization". . p. 7231 - 7234. Retrieved 2007/10/02.