3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID

Base Information

• Chemical Name: 3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID
• CAS No.: 152606-17-2
• Molecular Formula: C₉H₉Cl₂NO₂
• Molecular Weight: 234.082
• Hs Code.: 2922499990
• Mol file: 152606-17-2.mol

Synonyms:DL-3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID;3-(2,4-DICHLOROPHENYL)-BETA-ALANINE;3-AMINO-3-(2,4-DICHLOROPHENYL)PROPANOIC ACID;3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID;RARECHEM AK HW 0011;VITAS-BB TBB000139

Chemical Property of 3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID

Chemical Property:

• Vapor Pressure: 3.64E-06mmHg at 25°C
• Refractive Index: 1.6
• Boiling Point: 371.1°Cat760mmHg
• Flash Point: 178.3°C
• PSA: 63.32000
• Density: 1.447g/cm³
• LogP: 3.16820
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

99%, ^*data from raw suppliers

3-Amino-3-(2,4-dichlorophenyl)propanoicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID

There total 2 articles about 3-AMINO-3-(2,4-DICHLORO-PHENYL)-PROPIONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

malonic acid (141-82-2) + 2,4-dichlorobenzaldeyhde (874-42-0) → 3-amino-3-(2, 4-dichlorophenyl)propanoic acid (152606-17-2,778571-53-2)

Guidance literature:

With ammonium formate; In ethanol; for 7h; Reflux;

DOI:10.1016/j.ejmech.2017.11.065

Reference yield: 85.0%

→ 3-amino-3-(2, 4-dichlorophenyl)propanoic acid (152606-17-2,778571-53-2)

Guidance literature:

With ammonium formate; In ethanol; for 7h; Reflux;

Reference yield:

3-amino-3-(2, 4-dichlorophenyl)propanoic acid (152606-17-2,778571-53-2) → 3-(2, 4-dichlorophenyl)-3-((4-(trifluoromethyl)phenyl)sulfonamido)propanoic acid

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid / 7 h / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: water; lithium hydroxide / methanol / 4 h / 60 °C

With sulfuric acid; water; triethylamine; lithium hydroxide; In methanol; dichloromethane;

DOI:10.1016/j.ejmech.2017.11.065

upstream raw materials:

malonic acid

2,4-dichlorobenzaldeyhde

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