TETRADECYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: TETRADECYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE
• CAS No.: 152914-69-7
• Molecular Formula: C₂₂H₄₃NO₆
• Molecular Weight: 417.587
• Mol file: 152914-69-7.mol

Synonyms:TETRADECYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE;Tetradecyl2-acetamido-2-deoxy-b-D-glucopyranoside;TETRADECYL 2-ACETAMIDO-2-DEOXY-SS-D-GLUCOPYRANOSIDE

Chemical Property of TETRADECYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

• Boiling Point: 610.5±55.0 °C(Predicted)
• PKA: 13.00±0.70(Predicted)
• PSA: 108.25000
• Density: 1.09±0.1 g/cm3(Predicted)
• LogP: 3.03870

Purity/Quality:

98%,99%, ^*data from raw suppliers

TETRADECYL-2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRADECYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

There total 3 articles about TETRADECYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

n-tetradecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-dlucopyranoside (173725-25-2) → n-tetradecyl 2-acetamido-2-deoxy-β-D-glucopyranoside (152914-69-7)

Guidance literature:

With sodium methylate; for 16h; Ambient temperature;

DOI:10.1016/0008-6215(95)00229-1

Reference yield:

1-Tetradecanol (112-72-1) → n-tetradecyl 2-acetamido-2-deoxy-β-D-glucopyranoside (152914-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 62 percent / FeCl₃, 4A molecular sieves / CH₂Cl₂ / 10 h / Heating

2: 98 percent / methanol. NaOMe / 16 h / Ambient temperature

With 4 A molecular sieve; sodium methylate; iron(III) chloride; In dichloromethane;

DOI:10.1016/0008-6215(95)00229-1

Reference yield:

2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose (3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,76375-61-6,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3) → n-tetradecyl 2-acetamido-2-deoxy-β-D-glucopyranoside (152914-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 62 percent / FeCl₃, 4A molecular sieves / CH₂Cl₂ / 10 h / Heating

2: 98 percent / methanol. NaOMe / 16 h / Ambient temperature

With 4 A molecular sieve; sodium methylate; iron(III) chloride; In dichloromethane;

DOI:10.1016/0008-6215(95)00229-1

upstream raw materials:

n-tetradecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-dlucopyranoside

1-Tetradecanol

2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose