UROPORPHYRIN I ETHYL ESTER

Base Information

• Chemical Name: UROPORPHYRIN I ETHYL ESTER
• CAS No.: 54090-85-6
• Molecular Formula: C56H70N4O16
• Molecular Weight: 942.96
• Mol file: 54090-85-6.mol

Synonyms:UROPORPHYRIN I ETHYL ESTER;uroporphyrin I ethyl ester from*bovine porphyric;UROPORPHYRIN I ETHYL ESTER FROM*BOVINE P ORPHYRIC UR;uroporphyrin i ethyl ester from bovine porphyric urine

Chemical Property of UROPORPHYRIN I ETHYL ESTER

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.546
• Boiling Point: 1178.7°C at 760 mmHg
• Flash Point: 666.6°C
• PSA: 310.70000
• Density: 1.225g/cm³
• LogP: 2.44570
• Storage Temp.: −20°C

Purity/Quality:

98.5% ^*data from raw suppliers

Uroporphyrin I ethyl ester from bovine porphyric urine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of UROPORPHYRIN I ETHYL ESTER

There total 2 articles about UROPORPHYRIN I ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + ethyl 3-(4-ethoxycarbonylmethyl-1H-pyrrol-3-yl)-propionate (367967-01-9) → 3,3',3'',3'''-(3,7,13,17-tetrakis-ethoxycarbonylmethyl-porphyrin-2,8,12,18-tetrayl)-tetra-propionic acid tetraethyl ester (124360-23-2) + Oktacarbonsaeureuroporphyrinperaethylester (54090-85-6) + 3-[(1Z,4Z,9Z,15Z)-8,13,17-Tris-(2-ethoxycarbonyl-ethyl)-3,7,12,18-tetrakis-ethoxycarbonylmethyl-porphyrin-2-yl]-propionic acid ethyl ester + 3-[(1Z,5Z,9Z,14Z)-8,13,18-Tris-(2-ethoxycarbonyl-ethyl)-3,7,12,17-tetrakis-ethoxycarbonylmethyl-22,24-dihydro-porphin-2-yl]-propionic acid ethyl ester

Guidance literature:

formaldehyd; ethyl 3-(4-ethoxycarbonylmethyl-1H-pyrrol-3-yl)-propionate; With toluene-4-sulfonic acid; In benzene; for 4h; Heating;

With oxygen; In benzene; at 20 ℃; for 2h; Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(01)01160-1

Reference yield:

→ Oktacarbonsaeureuroporphyrinperaethylester (54090-85-6)

Guidance literature:

S.425;

DOI:10.1042/bj1610425

upstream raw materials:

formaldehyd

ethyl 3-(4-ethoxycarbonylmethyl-1H-pyrrol-3-yl)-propionate

Refernces

• 1、 With,Pedersen. "Molar absorption coefficients of porphyrin esters in chloroform determined by copper titration". . p. 425 - 429. Retrieved 2007/10/09.