1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI)

Base Information

Chemical Name:1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI)
CAS No.:500021-09-0
Molecular Formula:C₇H₁₂O₃
Molecular Weight:144.17
Hs Code.:
Mol file:500021-09-0.mol

Synonyms:1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI)

Suppliers and Price of 1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI)

Chemical Property:

PSA：35.53000
LogP:0.72690

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI)

There total 1 articles about 1,3-Dioxolane-4-carboxaldehyde, 2-ethyl-2-methyl-, (4R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 69-65-8
mannitol

: 78-93-3
butanone

: 500021-09-0
C₇H₁₂O₃

Guidance literature:: mannitol; butanone; With boron trifluoride diethyl etherate; orthoformic acid triethyl ester; In dimethyl sulfoxide; at 22 ℃; for 13h;

With sodium periodate; tetrabutyl ammonium fluoride; In diethyl ether; water; at 20 ℃; for 6h;
DOI:10.1021/ol300272j

Reference yield: 79.0%

: 500021-09-0
C₇H₁₂O₃

: 20913-05-7,859-65-4
(Benzoylmethylene)triphenylphosphorane

: 1360618-70-7
(E)-(4S)-3-(2-ethyl-2-methyl-[1,3]dioxolan-4-yl)-1-phenylprop-2-en-1-one

Guidance literature:: In tetrahydrofuran; for 9h; Reflux;
DOI:10.1021/ol300272j

Reference yield:

: 500021-09-0
C₇H₁₂O₃

: 1360618-79-6
(E)-(2S,3R,4R,5S)-(2-ethyl-5-hydroxy-2-methyl-4-styryltetrahydropyran-3-yl)phenylmethanone

: 1360618-80-9
(E)-(2R,3R,4R,5S)-(2-ethyl-5-hydroxy-2-methyl-4-styryltetrahydropyran-3-yl)phenylmethanone

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 9 h / Reflux

2: trifluoroacetic anhydride / dichloromethane / 18 h / 20 °C

With trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300272j