3-CHLORO-5-HYDROXYBENZALDEHYDE

Base Information

• Chemical Name: 3-CHLORO-5-HYDROXYBENZALDEHYDE
• CAS No.: 1829-33-0
• Molecular Formula: C7H5ClO2
• Molecular Weight: 156.569
• Hs Code.: 2913000090
• Mol file: 1829-33-0.mol

Synonyms:3-CHLORO-5-HYDROXYBENZALDEHYDE

Chemical Property of 3-CHLORO-5-HYDROXYBENZALDEHYDE

Chemical Property:

• PSA: 37.30000
• LogP: 1.85810
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

3-Chloro-5-hydroxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-CHLORO-5-HYDROXYBENZALDEHYDE

There total 2 articles about 3-CHLORO-5-HYDROXYBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3-chloro-5-hydroxybenzonitrile (473923-97-6) → 3-chloro-5-hydroxybenzaldehyde (1829-33-0)

Guidance literature:

With pyridine; sodium hypophosphite monohydrate; acetic acid; In water; at 50 ℃; for 1h; Inert atmosphere;

Reference yield: 25.0%

3-methoxy-5-chlorobenzaldehyde (164650-68-4) → 3-chloro-5-hydroxybenzaldehyde (1829-33-0)

Guidance literature:

3-methoxy-5-chlorobenzaldehyde; With boron tribromide; In dichloromethane; at 0 ℃; for 1.25h;

With water; In dichloromethane;

Reference yield: 97.0%

4-Amino-1-methylpiperidine (41838-46-4) + 3-chloro-5-hydroxybenzaldehyde (1829-33-0) → 3-chloro-5-{[(1-methylpiperidin-4-yl)amino]methyl}phenol

Guidance literature:

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 18.5h;

upstream raw materials:

3-methoxy-5-chlorobenzaldehyde

3-chloro-5-hydroxybenzonitrile

Downstream raw materials:

3-chloro-5-(2,2,2-trifluoroethoxy)benzaldehyde

Ph(3-Cl)(5-TMSO)-(R,S)CH(OTMS)CN

3-chloro-5-(2-fluoroethoxy)benzaldehyde

3-chloro-5-difluoromethoxybenzaldehyde

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