5-AMINO-3-IODO (1H)INDAZOLE

Base Information

• Chemical Name: 5-AMINO-3-IODO (1H)INDAZOLE
• CAS No.: 599183-36-5
• Molecular Formula: C7H6IN3
• Molecular Weight: 259.049
• Hs Code.: 2933990090
• Mol file: 599183-36-5.mol

Synonyms:5-AMINO-3-IODO (1H)INDAZOLE;5-AMINO-3-IODOINDAZOLE

Chemical Property of 5-AMINO-3-IODO (1H)INDAZOLE

Chemical Property:

• PSA: 54.70000
• LogP: 2.33090
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

3-iodo-1H-indazol-5-amine 95%-98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-AMINO-3-IODO (1H)INDAZOLE

There total 4 articles about 5-AMINO-3-IODO (1H)INDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl (3-iodo-1H-indazol-5-yl)carbamate (1338795-64-4) → 3-iodo-1H-indazol-5 -amine (599183-36-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.3390/molecules23082051

Reference yield: 82.0%

3-iodo-5-nitro-1H-indazole (70315-69-4) → 3-iodo-1H-indazol-5 -amine (599183-36-5)

Guidance literature:

With hydrogen iodide; at 90 ℃; for 2h;

DOI:10.1016/j.bmcl.2009.10.103

Reference yield:

5-nitroindazole (5401-94-5) → 3-iodo-1H-indazol-5 -amine (599183-36-5)

Guidance literature:

5-nitroindazole; With iodine; potassium hydroxide; In N,N-dimethyl-formamide; at 65 ℃; for 1h; Inert atmosphere;

With hydrogen iodide; In water; at 90 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.ejmech.2016.08.026

upstream raw materials:

3-iodo-5-nitro-1H-indazole

5-nitroindazole

tert-butyl (3-iodo-1H-indazol-5-yl)carbamate

(1H-indazol-5-yl)-carbamic acid tert-butyl ester

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