4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI)

Base Information

Chemical Name:4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI)
CAS No.:593286-22-7
Molecular Formula:C11H19N3O
Molecular Weight:209.29
Hs Code.:
Mol file:593286-22-7.mol

Synonyms:4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI)

Suppliers and Price of 4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI)

Chemical Property:

PSA：44.35000
LogP:0.92400

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI)

There total 3 articles about 4H-Imidazole,2-ethyl-4,4-dimethyl-5-(1-pyrrolidinyl)-,3-oxide(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123-75-1
pyrrolidine

: 593286-17-0
4,4-dimethyl-2-ethyl-4H-imidazole-5-carbonitrile 3-oxide

: 593286-22-7
2-ethyl-4,4-dimethyl-5-pyrrolidin-1-yl-4H-imidazole 3-oxide

Guidance literature:: In dichloromethane; at 20 ℃;

Reference yield:

: 593286-06-7
2-ethyl-4,5,5-trimethyl-2,5-dihydro-1H-imidazol-1-ol

: 593286-22-7
2-ethyl-4,4-dimethyl-5-pyrrolidin-1-yl-4H-imidazole 3-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / i-PrONO; Et₃N / CH₂Cl₂ / 5 h

2: 85 percent / TsCl; Et₃N / CHCl₃ / 1 h

3: 90 percent / CH₂Cl₂ / 20 °C

With i-propyl nitrite; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; chloroform;

Reference yield:

: 4,4-dimethyl-2-ethyl-4H-imidazole-5-carbaldehyde oxime 3-oxide

: 593286-22-7
2-ethyl-4,4-dimethyl-5-pyrrolidin-1-yl-4H-imidazole 3-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / TsCl; Et₃N / CHCl₃ / 1 h

2: 90 percent / CH₂Cl₂ / 20 °C

With triethylamine; p-toluenesulfonyl chloride; In dichloromethane; chloroform;