9H-Pyrrolo[3,2,1-ij]quinolin-9-one,6a-ethyldecahydro-,(6aR,9aR,9bS)-rel-(9CI)

Base Information

• Chemical Name: 9H-Pyrrolo[3,2,1-ij]quinolin-9-one,6a-ethyldecahydro-,(6aR,9aR,9bS)-rel-(9CI)
• CAS No.: 502614-34-8
• Molecular Formula: C13H21NO
• Molecular Weight: 207.31
• Mol file: 502614-34-8.mol

Synonyms:9H-Pyrrolo[3,2,1-ij]quinolin-9-one,6a-ethyldecahydro-,(6aR,9aR,9bS)-rel-(9CI)

Chemical Property of 9H-Pyrrolo[3,2,1-ij]quinolin-9-one,6a-ethyldecahydro-,(6aR,9aR,9bS)-rel-(9CI)

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Technology Process of 9H-Pyrrolo[3,2,1-ij]quinolin-9-one,6a-ethyldecahydro-,(6aR,9aR,9bS)-rel-(9CI)

There total 158 articles about 9H-Pyrrolo[3,2,1-ij]quinolin-9-one,6a-ethyldecahydro-,(6aR,9aR,9bS)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C15H25NO2 → (6aα,9aβ,9bβ)-6a-ethyldecahydro-4H-pyrrolo[3,2,1-i,j]quinolin-9-one (502614-34-8,502614-35-9)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 80 ℃; for 1h;

DOI:10.1002/anie.200701943

Reference yield: 88.0%

methyl (6aRS,9aSR,9bRS)-6a-ethyl-octahydro-9-oxo-1H-pyrrolo[3,2,1-ij]quinoline-9a-carboxylate → (6aα,9aβ,9bβ)-6a-ethyldecahydro-4H-pyrrolo[3,2,1-i,j]quinolin-9-one (502614-34-8,502614-35-9)

Guidance literature:

With lithium chloride; In N,N-dimethyl-formamide; at 140 ℃; for 3h;

DOI:10.1021/ol052749q

Reference yield: 85.0%

C19H23NOS → (6aα,9aβ,9bβ)-6a-ethyldecahydro-4H-pyrrolo[3,2,1-i,j]quinolin-9-one (502614-34-8,502614-35-9)

Guidance literature:

With Raney nickel; In ethanol; at 20 ℃; for 12h;

DOI:10.1039/b903530c

upstream raw materials:

C₁₈H₃₂INO₂

C₁₈H₃₁NO₂

C₁₈H₃₁NO₅

C₁₉H₃₃NO₅

Downstream raw materials:

(+)-deacetylaspidospermine

(-)-N-acetylaspidospermidine

(-)-pyrifolidine

(-)-demethoxypalosine

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