10H-Benzo(b)xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate

Base Information

• Chemical Name: 10H-Benzo(b)xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate
• CAS No.: 33390-28-2
• Molecular Formula: C₂₄H₁₈O₁₀
• Molecular Weight: 466.401
• DSSTox Substance ID: DTXSID40187021
• Nikkaji Number: J69.862H
• Wikidata: Q83058536
• Mol file: 33390-28-2.mol

Synonyms:Diacetyl-O-bikaverin;BRN 1444530;33390-28-2;10H-Benzo(b)xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate;10H-Benzo[b]xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate;DTXSID40187021;C24H18O10;C24-H18-O10;LS-41594;(6-Acetyloxy-3,8-dimethoxy-1-methyl-7,10,12-trioxobenzo[b]xanthen-11-yl)acetate;10H-Benzo[b]xanthene-7,8,12-trione, 6,11-bis(acetyloxy)-3,8-dimethoxy-1-methyl-

Chemical Property of 10H-Benzo(b)xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate

Chemical Property:

• Vapor Pressure: 1.05E-19mmHg at 25°C
• Boiling Point: 704.7°C at 760 mmHg
• Flash Point: 303.5°C
• PSA: 135.41000
• Density: 1.49g/cm³
• LogP: 3.02310
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 6
• Exact Mass: 466.08999677
• Heavy Atom Count: 34
• Complexity: 938

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=CC2=C1C(=O)C3=C(O2)C(=C4C(=C3OC(=O)C)C(=O)C=C(C4=O)OC)OC(=O)C)OC

Technology Process of 10H-Benzo(b)xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate

There total 3 articles about 10H-Benzo(b)xanthene-7,10,12-trione, 6,11-dihydroxy-3,8-dimethoxy-1-methyl-, diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridine (110-86-1) + 7,10-dihydroxy-3,8-dimethoxy-1-methyl-1H-benzo[b]xanthene-6,11,12-trione + acetic anhydride (108-24-7) → Acetic acid 7-acetoxy-3,8-dimethoxy-1-methyl-6,11,12-trioxo-6,12-dihydro-11H-benzo[b]xanthen-10-yl ester (33390-29-3) + Acetic acid 11-acetoxy-3,8-dimethoxy-1-methyl-7,10,12-trioxo-7,12-dihydro-10H-benzo[b]xanthen-6-yl ester (33390-28-2)

Guidance literature:

Reference yield:

perchloric acid (7601-90-3) + 7,10-dihydroxy-3,8-dimethoxy-1-methyl-1H-benzo[b]xanthene-6,11,12-trione + acetic anhydride (108-24-7) → Acetic acid 7-acetoxy-3,8-dimethoxy-1-methyl-6,11,12-trioxo-6,12-dihydro-11H-benzo[b]xanthen-10-yl ester (33390-29-3) + Acetic acid 11-acetoxy-3,8-dimethoxy-1-methyl-7,10,12-trioxo-7,12-dihydro-10H-benzo[b]xanthen-6-yl ester (33390-28-2)

Guidance literature:

Reference yield:

→ Acetic acid 11-acetoxy-3,8-dimethoxy-1-methyl-7,10,12-trioxo-7,12-dihydro-10H-benzo[b]xanthen-6-yl ester (33390-28-2)

Guidance literature:

Bikaverin I, Acetanhydrid (sowie Perchlors.);

upstream raw materials:

pyridine

acetic anhydride

perchloric acid