N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride

Base Information

Chemical Name:N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride
CAS No.:55246-78-1
Molecular Formula:C₉H₁₀ClNS
Molecular Weight:199.704
Hs Code.:2930909090
European Community (EC) Number:670-601-6
DSSTox Substance ID:DTXSID90374964
Wikidata:Q82163523
Mol file:55246-78-1.mol

Synonyms:55246-78-1;N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride;N-methyl-N-(4-methylphenyl)carbamothioyl chloride;Methyl(p-tolyl)carbamothioic chloride;DTXSID90374964;Methyl(p-tolyl)carbamothioicchloride;MFCD03093781;AKOS006276941;N-methyl-N-(p-tolyl)carbamothioyl chloride;N-(chloromethanethioyl)-N,4-dimethylaniline;FT-0640297;A830554

Suppliers and Price of N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl(p-tolyl)carbamothioicchloride 97%
25g
$ 383.00

American Custom Chemicals Corporation
N-METHYL-N-(4-METHYLPHENYL)THIOCARBAMOYL CHLORIDE 95.00%
5G
$ 928.97

Total 5 raw suppliers

Chemical Property of N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride

Chemical Property:

Vapor Pressure:0.00367mmHg at 25°C
Melting Point:56 °C
Refractive Index:1.638
Boiling Point:281°C at 760 mmHg
Flash Point:123.7°C
PSA：35.33000
Density:1.247g/cm³
LogP:2.95490
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:199.0222482
Heavy Atom Count:12
Complexity:164

Purity/Quality:

98%min ^*data from raw suppliers

Methyl(p-tolyl)carbamothioicchloride 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N(C)C(=S)Cl

Technology Process of N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride

There total 1 articles about N-Methyl-N-(4-methylphenyl)thiocarbamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 463-71-8
thiophosgene

: 623-08-5
N-methyl-p-toluidine

: 55246-78-1
methyl(p-tolyl)carbamothioic chloride

Guidance literature:: With diethyl ether;

Reference yield:

: 55246-78-1
methyl(p-tolyl)carbamothioic chloride

: 1415351-70-0
S-but-3-en-2-yl methyl(p-tolyl)carbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride; sodium iodide / tetrahydrofuran / Inert atmosphere

2: toluene / Reflux; Inert atmosphere

With sodium hydride; sodium iodide; In tetrahydrofuran; toluene;
DOI:10.1021/ol5002522

Reference yield:

: 55246-78-1
methyl(p-tolyl)carbamothioic chloride

: 1558811-69-0
S-2-p-tolylbut-3-en-2-yl methylcarbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride; sodium iodide / tetrahydrofuran / Inert atmosphere

2.1: toluene / Reflux; Inert atmosphere

3.1: lithium diisopropyl amide; lithium chloride / tetrahydrofuran / 2 h / -60 °C / Inert atmosphere

3.2: 0.17 h / -78 °C / Inert atmosphere

With sodium hydride; sodium iodide; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1021/ol5002522