2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI)

Base Information

Chemical Name:2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI)
CAS No.:50771-95-4
Molecular Formula:C₈H₇ClN₂S
Molecular Weight:198.676
Hs Code.:
Mol file:50771-95-4.mol

Synonyms:2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI)

Suppliers and Price of 2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI)

Chemical Property:

Boiling Point:300.3±44.0 °C(Predicted)
PKA:10.57±0.30(Predicted)
Density:1.47±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI)

There total 1 articles about 2H-Benzimidazole-2-thione,7-chloro-1,3-dihydro-1-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75335-72-7
4-chloro-1,3-dihydro-2H-benzo[d]imidazole-2-thione

: 76-83-5
trityl chloride

: 74-88-4
methyl iodide

: 4-chloro-1-methyl-1,3-dihydro-2H-benzo[d]imidazole-2-thione

: 50771-95-4
7-chloro-1-methyl-1,3-dihydro-2H-benzo[d]imidazole-2-thione

Guidance literature:: 4-chloro-1,3-dihydro-2H-benzo[d]imidazole-2-thione; trityl chloride; With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With potassium hydroxide; In acetone; at 20 ℃; for 0.05h; Inert atmosphere;

methyl iodide; regioselective reaction; Further stages;
DOI:10.1016/j.tetlet.2019.151078