[1,1-Biphenyl]-3-ol,6-methyl-(9CI)

Base Information

• Chemical Name: [1,1-Biphenyl]-3-ol,6-methyl-(9CI)
• CAS No.: 50715-86-1
• Molecular Formula: C13H12O
• Molecular Weight: 184.23
• Hs Code.: 2907199090
• Mol file: 50715-86-1.mol

Synonyms:[1,1-Biphenyl]-3-ol,6-methyl-(9CI)

Chemical Property of [1,1-Biphenyl]-3-ol,6-methyl-(9CI)

Chemical Property:

• PSA: 20.23000
• LogP: 3.36760

Purity/Quality:

6-Methyl-[1,1'-biphenyl]-3-ol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [1,1-Biphenyl]-3-ol,6-methyl-(9CI)

There total 6 articles about [1,1-Biphenyl]-3-ol,6-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-bromo-p-cresol (60710-39-6) + phenylboronic acid (98-80-6) → 4-methyl-3-phenylphenol (50715-86-1)

Guidance literature:

3-bromo-p-cresol; phenylboronic acid; With potassium carbonate; In 1,4-dioxane; water; for 0.5h; Inert atmosphere;

With bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; water; for 16h; Reflux; Inert atmosphere;

DOI:10.1021/acs.joc.1c02459

Reference yield: 88.0%

6-methyl-5,6-dihydro-[1,1'-biphenyl]-3(4H)-one (16735-15-2,67648-93-5) → 4-methyl-3-phenylphenol (50715-86-1)

Guidance literature:

With hydrogen bromide; oxygen; copper(ll) bromide; In 1,4-dioxane; water; at 20 ℃; for 20h; Sealed tube;

DOI:10.1039/c3ra43071e

Reference yield:

4-methyl-4-phenyl-cyclohex-2,5-dien-1-one (28937-18-0) → 4-methyl-3-phenylphenol (50715-86-1)

Guidance literature:

With trifluoroacetic acid; In water; at 38.5 ℃; Rate constant;

DOI:10.1021/ja00814a022

upstream raw materials:

4-hydroxy-4-methyl-5-phenyl-cyclohex-2-enone

4-methyl-4-phenyl-cyclohex-2,5-dien-1-one

6-methyl-5,6-dihydro-[1,1'-biphenyl]-3(4H)-one

3-bromo-p-cresol

Downstream raw materials:

5-methoxy-[1,1′-biphenyl]-2-carboxylic acid

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