Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI)

Base Information

Chemical Name:Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI)
CAS No.:499196-14-4
Molecular Formula:C14H19NO
Molecular Weight:217.30676
Hs Code.:
Mol file:499196-14-4.mol

Synonyms:Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI)

Suppliers and Price of Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI)

There total 3 articles about Isoquinoline, 2-acetyl-4-ethyl-1,2,3,4-tetrahydro-3-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 255713-86-1
N-benzyl-N-(1-cyclopropylethyl)acetamide

: 499196-14-4
N-acetyl-4-ethyl-3-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With PPA; at 70 ℃; for 6h;
DOI:10.1081/SCC-120012985

Reference yield:

: 129297-33-2
N-benzyl-N-(1-cyclopropylethylidene)amine

: 499196-14-4
N-acetyl-4-ethyl-3-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaBH₄ / methanol / 25 °C

2: 80 percent / polyphosphoric acid / 6 h / 70 °C

With sodium tetrahydroborate; PPA; In methanol; 3: Friedel-Crafts alkylation;
DOI:10.1081/SCC-120012985

Reference yield:

: 133612-01-8
N-benzyl-N-(1-cyclopropylethyl)amine

: 499196-14-4
N-acetyl-4-ethyl-3-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / polyphosphoric acid / 6 h / 70 °C

With PPA; 2: Friedel-Crafts alkylation;
DOI:10.1081/SCC-120012985