3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI)

Base Information

Chemical Name:3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI)
CAS No.:499781-64-5
Molecular Formula:C10H16O
Molecular Weight:152.23344
Hs Code.:
Mol file:499781-64-5.mol

Synonyms:3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI)

Suppliers and Price of 3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI)

There total 3 articles about 3-Cyclohexen-1-one, 3-methyl-6-(1-methylethyl)-, (6S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 499781-62-3
(6S)-6-isopropyl-3-methylcyclohex-3-en-1-ol

: 499781-64-5
(6S)-3-methyl-6-isopropylcyclohex-3-en-1-one

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -60 - 20 ℃;
DOI:10.1081/SCC-120012982

Reference yield:

: 499781-61-2
(6S)-6-isopropenyl-3-methylcyclohex-3-en-1-ol

: 499781-64-5
(6S)-3-methyl-6-isopropylcyclohex-3-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney-Ni / ethanol / 20 °C / 760 Torr

2: CrO₃, H₂SO₄

With chromium(VI) oxide; sulfuric acid; hydrogen; nickel; In ethanol;

Reference yield:

: (Z)-(5S)-6-hydroxy-5-isopropyl-2-methylcyclohex-2-ene p-toluenesulfonylhydrazone

: 499781-64-5
(6S)-3-methyl-6-isopropylcyclohex-3-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium borohydride / 2-methyl-propan-2-ol / 1 h / Heating

2: 70 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -60 - 20 °C

With sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; tert-butyl alcohol; 2: Swern oxidation;
DOI:10.1081/SCC-120012982