3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI)

Base Information

Chemical Name:3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI)
CAS No.:499781-61-2
Molecular Formula:C10H16O
Molecular Weight:152.236
Hs Code.:
Mol file:499781-61-2.mol

Synonyms:3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI)

Suppliers and Price of 3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI)

Chemical Property:

PSA：20.23000
LogP:2.27970

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI)

There total 2 articles about 3-Cyclohexen-1-ol, 3-methyl-6-(1-methylethenyl)-, (6S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 499781-54-3
(Z)-(5S,6S)-(-)-6-hydroxy-5-isopropenyl-2-methylcyclohex-2-ene p-toluenesulfonylhydrazone

: 499781-61-2
(6S)-6-isopropenyl-3-methylcyclohex-3-en-1-ol

Guidance literature:: With sodium tetrahydroborate; In tert-butyl alcohol; for 1h; Heating;
DOI:10.1081/SCC-120012982

Reference yield:

: 510753-48-7
(R)-carvone p-tolylsulphonylhydrazone

: 499781-61-2
(6S)-6-isopropenyl-3-methylcyclohex-3-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N',N'-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C

1.2: N,N,N',N'-tetramethylethylenediamine; O₂ / hexane; tetrahydrofuran / 7 h / 20 °C

2.1: 83 percent / sodium borohydride / 2-methyl-propan-2-ol / 1 h / Heating

With sodium tetrahydroborate; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; tert-butyl alcohol;
DOI:10.1081/SCC-120012982