1,6-Bis(methylsulfonylsulfanyl)hexane

Base Information

• Chemical Name: 1,6-Bis(methylsulfonylsulfanyl)hexane
• CAS No.: 56-01-9
• Molecular Formula: C8H18O4S4
• Molecular Weight: 306.493
• Hs Code.: 2930909090
• DSSTox Substance ID: DTXSID20391785
• Nikkaji Number: J1.425.109J
• Mol file: 56-01-9.mol

Synonyms:1,6-bis(methylsulfonylsulfanyl)hexane;56-01-9;1,6-Hexanedithiol Dimethanesulfonate;Methanesulfonothioic Acid S,S'-1,6-Hexanediyl Ester;DTXSID20391785;Hexamethylenebisthiobis(methyl sulfone);FT-0669192

Chemical Property of 1,6-Bis(methylsulfonylsulfanyl)hexane

Chemical Property:

• Melting Point: 81-82°C
• Boiling Point: 533.8oC at 760 mmHg
• Flash Point: 276.7oC
• PSA: 135.64000
• Density: 1.329g/cm3
• LogP: 4.09400
• Storage Temp.: -20°C Freezer
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 9
• Exact Mass: 306.00879375
• Heavy Atom Count: 16
• Complexity: 322

Purity/Quality:

98%Min ^*data from raw suppliers

1,6-HexanediylBismethanethiosulfonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CS(=O)(=O)SCCCCCCSS(=O)(=O)C
• Uses: A sulfhydryl cross-linking reagent A sulfhydryl cross-linking reagent.

Technology Process of 1,6-Bis(methylsulfonylsulfanyl)hexane

There total 2 articles about 1,6-Bis(methylsulfonylsulfanyl)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1 ,6-dibromohexane (629-03-8) + ammonium methanethiosulphonate → S,S'-hexamethylene-bis(methanethiosulphonate) (56-01-9)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; at 60 ℃; for 3h;

Reference yield:

1 ,6-dibromohexane (629-03-8) + sodium methanethiosulfonate (1950-85-2) → S,S'-hexamethylene-bis(methanethiosulphonate) (56-01-9)

Guidance literature:

In ethanol; Heating;

DOI:10.1248/cpb.12.1271

Reference yield:

S,S'-hexamethylene-bis(methanethiosulphonate) (56-01-9) → 1,6-dimercaptohexane (1191-43-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1h; Heating;

upstream raw materials:

1 ,6-dibromohexane

sodium methanethiosulfonate

Downstream raw materials:

1,6-dimercaptohexane