3-Naphthalen-1-yl-benzaldehyde

Base Information

• Chemical Name: 3-Naphthalen-1-yl-benzaldehyde
• CAS No.: 56432-20-3
• Molecular Formula: C17H12O
• Molecular Weight: 232.282
• DSSTox Substance ID: DTXSID70971859
• Nikkaji Number: J2.001.557H
• Wikidata: Q82955509

Synonyms:3-Naphthalen-1-yl-benzaldehyde;56432-20-3;3-naphthalen-1-ylbenzaldehyde;3-(1-naphthyl)benzaldehyde;3-(NAPHTHALEN-1-YL)BENZALDEHYDE;3-(1-Naphthalenyl)benzaldehyde;SCHEMBL7569927;DTXSID70971859;CAXHDVXIZDLPBE-UHFFFAOYSA-N

Chemical Property of 3-Naphthalen-1-yl-benzaldehyde

Chemical Property:

• PSA: 17.07000
• LogP: 4.31930
• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 232.088815002
• Heavy Atom Count: 18
• Complexity: 285

Purity/Quality:

98%min ^*data from raw suppliers

3-(2-Hydroxynaphthalen-1-yl)benzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2C3=CC=CC(=C3)C=O

Technology Process of 3-Naphthalen-1-yl-benzaldehyde

There total 3 articles about 3-Naphthalen-1-yl-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

dinaphthalen-1-ylzinc (7029-32-5) + 3-bromobenzaldehyde diethylacetal (75148-49-1) → 1-(3-formylphenyl)-naphthalene (56432-20-3)

Guidance literature:

With dichloro{bis[1-(dicyclohexylphosphanyl)piperidine]}palladium(II); In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 100 ℃; for 0.0833333h; In air;

DOI:10.1002/chem.201001201

Reference yield: 80.0%

m-bromobenzoic aldehyde (3132-99-8) + 1-Naphthylboronic acid (13922-41-3) → 1-(3-formylphenyl)-naphthalene (56432-20-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 10h;

DOI:10.1016/j.tetlet.2009.01.027

Reference yield: 72.0%

1-Naphthalenesulfonyl chloride (85-46-1) + 3-Formylphenylboronic acid (87199-16-4) → 1,1'-bisnaphthalene (604-53-5) + 1-(3-formylphenyl)-naphthalene (56432-20-3)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; sodium carbonate; 1,3-bis(mesityl)imidazolium chloride; In tetrahydrofuran; Heating;

DOI:10.1021/ol036131x

upstream raw materials:

1-Naphthalenesulfonyl chloride

3-Formylphenylboronic acid

m-bromobenzoic aldehyde

1-Naphthylboronic acid

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