Technology Process of 1H-Indole-3-aceticacid,5-amino-(9CI)
There total 7 articles about 1H-Indole-3-aceticacid,5-amino-(9CI) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydrogen;
palladium on activated charcoal;
In
water;
for 1.66667h;
under 2327.2 Torr;
Ambient temperature;
DOI:10.1016/0031-9422(80)85060-6
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 91 percent / Br2 / acetic acid
2: 91 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 6 h / Heating
3: 91 percent / acetic acid / 7 h / 70 °C
5: 92 percent / conc. HCl / 6 h / Heating
6: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
With
hydrogenchloride; potassium hydroxide; hydrogen; bromine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
palladium on activated charcoal;
In
water; acetic acid; benzene;
DOI:10.1016/0031-9422(80)85060-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 6 h / Heating
2: 91 percent / acetic acid / 7 h / 70 °C
4: 92 percent / conc. HCl / 6 h / Heating
5: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
With
hydrogenchloride; potassium hydroxide; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
palladium on activated charcoal;
In
water; acetic acid; benzene;
DOI:10.1016/0031-9422(80)85060-6