Technology Process of trans-2,3-Epoxynonane
There total 8 articles about trans-2,3-Epoxynonane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H32O4S;
With
5%-palladium/activated carbon; hydrogen;
In
methanol;
at 22 ℃;
for 5h;
under 760.051 Torr;
With
potassium carbonate;
In
methanol;
at 22 ℃;
for 1.5h;
DOI:10.1021/ja405151n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: p-TsOH, molacular sieves 4 Angstroem / CH2Cl2 / Ambient temperature
2: 1.) chiral cyclic -C(Bn)-C(O)-O-B(Ph)-N(Ts)-, t-BuSC(CH2)OTMS; 2.) CH3SO2Cl, Et3N; 3.) potassium acetate / 1.) CH2Cl2, -78 deg C, 15 h; 2.) CH2Cl2, rt.; 3.) DMF, 85 deg C
With
t-BuSC(CH2)OTMS; potassium acetate; toluene-4-sulfonic acid; methanesulfonyl chloride; triethylamine;
In
dichloromethane;
DOI:10.1016/S0040-4039(98)02387-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: baker's yeast / H2O / 48 h / 33 °C / pH 7-5
2: MeONa
With
baker's yeast; sodium methylate;
In
water;
DOI:10.1016/S0040-4039(00)85052-2
