Technology Process of Ethanone, 2,2-dichloro-1-(2-methoxyphenyl)- (9CI)
There total 4 articles about Ethanone, 2,2-dichloro-1-(2-methoxyphenyl)- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
N,N-dimethyl acetamide;
at 25 ℃;
for 0.5h;
under 760.051 Torr;
chemoselective reaction;
DOI:10.1002/adsc.201100778
- Guidance literature:
-
With
chloroform; water; lithium perchlorate; tetra-(n-butyl)ammonium iodide;
In
acetonitrile;
at 20 ℃;
for 6h;
Electrochemical reaction;
DOI:10.1021/acs.orglett.0c00052
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform / 27 h / Inert atmosphere
2.1: sodium dichromate; sulfuric acid / acetic acid / 0.17 h / 20 °C
2.2: 0.17 h
3.1: palladium 10% on activated carbon; hydrogen / N,N-dimethyl acetamide / 0.5 h / 25 °C / 760.05 Torr
With
sulfuric acid; palladium 10% on activated carbon; sodium dichromate; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
chloroform; N,N-dimethyl acetamide; acetic acid;
DOI:10.1002/adsc.201100778
