Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI)
CAS No.:53821-16-2
Molecular Formula:C14H12N2O4
Molecular Weight:272.26
Hs Code.:2924299090
Mol file:53821-16-2.mol

Synonyms:Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI)

Suppliers and Price of Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(3-NITROPHENYL)-CARBAMIC ACID PHENYLMETHYL ESTER 95.00%
5MG
$ 497.87

Total 1 raw suppliers

Chemical Property of Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI)

Chemical Property:

PSA：84.15000
LogP:3.93970

Purity/Quality:: (3-NITROPHENYL)-CARBAMIC ACID PHENYLMETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI)

There total 9 articles about Carbamic acid, (3-nitrophenyl)-, phenylmethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124-38-9,18923-20-1
carbon dioxide

: 100-44-7
benzyl chloride

: 99-09-2
3-nitro-aniline

: 53821-16-2
(3-nitrophenyl)carbamic acid benzyl ester

Guidance literature:: carbon dioxide; 3-nitro-aniline; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 1h;

benzyl chloride; In N,N-dimethyl-formamide; at 23 ℃; for 120h;
DOI:10.1016/S0040-4020(02)00286-7

Reference yield: 92.8%

: 501-53-1,94274-21-2
benzyl chloroformate

: 99-09-2
3-nitro-aniline

: 53821-16-2
(3-nitrophenyl)carbamic acid benzyl ester

Guidance literature:: In PEG-600; at 20 ℃; for 0.166667h; chemoselective reaction;
DOI:10.1016/j.cclet.2012.05.012

Reference yield: 59.0%

: 3320-87-4
isocyanic acid (3-nitro-phenyl) ester

: 62673-31-8
benzyl(bromo)zinc

: 53821-16-2
(3-nitrophenyl)carbamic acid benzyl ester

Guidance literature:: isocyanic acid (3-nitro-phenyl) ester; benzyl(bromo)zinc; In tetrahydrofuran; at 55 ℃; for 8h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.053