Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI)

Base Information

Chemical Name:Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI)
CAS No.:632322-81-7
Molecular Formula:C10H18O2
Molecular Weight:170.25
Hs Code.:
Mol file:632322-81-7.mol

Synonyms:Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI)

Suppliers and Price of Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI)

Chemical Property:

Purity/Quality:

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Technology Process of Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI)

There total 4 articles about Benzofuran, octahydro-2-methoxy-2-methyl-, (3aR,7aR)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 186586-89-0
2-(2-methoxy-1-propene-3-yl)cyclohexanol

: 186586-84-5,632322-81-7
8-methoxy-8-methyl-7-oxabicyclo<4.3.0>heptane

Guidance literature:: In tetrachloromethane; for 0.166667h; Heating;
DOI:10.1002/cber.19971300107

Reference yield: 72.0%

: 632322-78-2
3-(2-Bromo-1-methoxy-1-methyl-ethoxy)-cyclohexene

: 186586-84-5,632322-81-7
8-methoxy-8-methyl-7-oxabicyclo<4.3.0>heptane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;
DOI:10.1039/c39950000469

Reference yield:

: 822-67-3
Cyclohex-2-enol

: 186586-84-5,632322-81-7
8-methoxy-8-methyl-7-oxabicyclo<4.3.0>heptane

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / N-bromosuccinimide / CH₂Cl₂ / 1.75 h / -50 - 20 °C

2: 72 percent / n-Bu₃SnH; AIBN / benzene / 2.5 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In dichloromethane; benzene;
DOI:10.1016/S0957-4166(03)00535-4