3-Pyridinamine,N-(2-furanylmethyl)-(9CI)

Base Information

• Chemical Name: 3-Pyridinamine,N-(2-furanylmethyl)-(9CI)
• CAS No.: 510703-88-5
• Molecular Formula: C10H10N2O
• Molecular Weight: 174.2
• Mol file: 510703-88-5.mol

Synonyms:3-Pyridinamine,N-(2-furanylmethyl)-(9CI)

Chemical Property of 3-Pyridinamine,N-(2-furanylmethyl)-(9CI)

Chemical Property:

• PSA: 38.06000
• LogP: 2.35970

Purity/Quality:

99% ^*data from raw suppliers

N-(furan-2-ylmethyl)pyridin-3-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Pyridinamine,N-(2-furanylmethyl)-(9CI)

There total 5 articles about 3-Pyridinamine,N-(2-furanylmethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-Chloropyridine (626-60-8) + furan-2-ylmethanamine (617-89-0) → N-(furan-2-ylmethyl)pyridin-3-amine (510703-88-5)

Guidance literature:

With bis{1,1’-diphenyl-3,3’-methylenediimidazoline-2,2’-diylidene}nickel(II) dibromide; potassium tert-butylate; In 1,4-dioxane; at 90 ℃; for 4h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2016.12.029

Reference yield: 98.0%

furan-2-ylmethanamine (617-89-0) + pyridin-3-yl trifluoromethanesulfonate (107658-27-5) → N-(furan-2-ylmethyl)pyridin-3-amine (510703-88-5)

Guidance literature:

With [COD(Pd-AlPhos)₂]; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tert-butyl methyl ether; at 60 ℃; for 16h; Inert atmosphere; Sealed tube; Schlenk technique;

DOI:10.1021/jacs.8b01696

Reference yield: 91.0%

3-Bromopyridine (626-55-1,163928-56-1) + furan-2-ylmethanamine (617-89-0) → N-(furan-2-ylmethyl)pyridin-3-amine (510703-88-5)

Guidance literature:

With potassium phosphate; copper(l) iodide; N,N-diethylsalicylamide; In N,N-dimethyl-formamide; at 90 ℃; for 20h;

DOI:10.1021/ol0273396

upstream raw materials:

3-Bromopyridine

furan-2-ylmethanamine

3-(2-furoyl)amino-pyridine-2-phosphonic acid diethyl ester

N,N-dimethyl-formamide dimethyl acetal

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