1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI)

Base Information

Chemical Name:1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI)
CAS No.:624746-79-8
Molecular Formula:C7H9BrN2O
Molecular Weight:217.06
Hs Code.:
Mol file:624746-79-8.mol

Synonyms:1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI)

Suppliers and Price of 1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI)

Chemical Property:

PSA：34.89000
LogP:1.78640

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI)

There total 1 articles about 1H-Imidazole-2-carboxaldehyde,5-bromo-1-ethyl-4-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624746-78-7
1-ethyl-5-methyl-1H-imidazole-2-carbaldehyde

: 624746-77-6
1-ethyl-4-methyl-1H-imidazole-2-carbaldehyde

: 624746-79-8
5-bromo-1-ethyl-4-methyl-1H-imidazole-2-carbaldehyde

: 624746-80-1
4-bromo-1-ethyl-5-methyl-1H-imidazole-2-carbaldehyde

Guidance literature:: With N-Bromosuccinimide; In acetonitrile; at 20 ℃; for 4h;

Reference yield:

: 624746-79-8
5-bromo-1-ethyl-4-methyl-1H-imidazole-2-carbaldehyde

: 16419-60-6
2-Methylphenylboronic acid

: 1-ethyl-4-methyl-5-(2-methylphenyl)-1H-imidazole-2-carbaldehyde

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 24h; Heating / reflux;

Reference yield:

: 624746-79-8
5-bromo-1-ethyl-4-methyl-1H-imidazole-2-carbaldehyde

: 2-[1-(1-ethyl-4-methyl-5-o-tolyl-1H-imidazol-2-ylmethyl)-1H-imidazol-2-yl]-6-fluoropyridine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 24 h / Heating / reflux

2: sodium tetrahydroborate / methanol / 3 h / 20 °C

3: thionyl chloride / dichloromethane / 4 h / 20 °C

4: potassium carbonate / DMF (N,N-dimethyl-formamide) / 24 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; toluene;