(3,5-Dimethylphenyl)phosphane

Base Information

Chemical Name:(3,5-Dimethylphenyl)phosphane
CAS No.:524695-90-7
Molecular Formula:C8H11P
Molecular Weight:138.149
Hs Code.:
DSSTox Substance ID:DTXSID90402635
Wikidata:Q82206064
Mol file:524695-90-7.mol

Synonyms:(3,5-DIMETHYLPHENYL)PHOSPHINE;524695-90-7;(3,5-dimethylphenyl)phosphane;3,5-Xylylphosphine;SCHEMBL5044874;DTXSID90402635;AKOS006295439;FT-0750135;3-AMINO-3-(2-HYDROXY-3-METHYL-PHENYL)-PROPIONICACID

Suppliers and Price of (3,5-Dimethylphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3,5-XYLYLPHOSPHINE 98.00%
50G
$ 3280.20

Total 3 raw suppliers

Chemical Property of (3,5-Dimethylphenyl)phosphane

Chemical Property:

PSA：13.59000
LogP:1.80380
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:138.059837349
Heavy Atom Count:9
Complexity:80.6

Purity/Quality:

98%Min ^*data from raw suppliers

3,5-XYLYLPHOSPHINE 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)P)C

Technology Process of (3,5-Dimethylphenyl)phosphane

There total 2 articles about (3,5-Dimethylphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 207513-05-1
dichloro(3,5-dimethylphenyl)phosphine

: 524695-90-7
3,5-di-methylphenylphosphine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/ja021224f

Reference yield:

: 556-96-7
5-bromo-1,3-xylene

: 524695-90-7
3,5-di-methylphenylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / tetrahydrofuran; hexane / -78 - 0 °C

1.2: ZnCl₂ / tetrahydrofuran; hexane / -78 °C

1.3: PCl₃ / tetrahydrofuran; hexane / -78 - 20 °C

2.1: LiAlH₄ / tetrahydrofuran; hexane / -78 - 20 °C

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/ja021224f

Reference yield: 71.0%

: 232923-64-7
(1S,5S)-5-((2'S)-1'-hydroxyprop-2'-yl)-2,2-dimethyl-1-cylcopentanol cyclic sulfate

: 524695-90-7
3,5-di-methylphenylphosphine

: (1R,2R,4S,5S)-4,8,8-trimethyl-2-(3',5'-dimethylphenyl)-2-phosphabicyclo[3.3.0]octane borane complex

Guidance literature:: 3,5-di-methylphenylphosphine; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.0833333h;

(1S,5S)-5-((2'S)-1'-hydroxyprop-2'-yl)-2,2-dimethyl-1-cylcopentanol cyclic sulfate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4.3h;

With borane-THF; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ja021224f