1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one

Base Information

Chemical Name:1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one
CAS No.:531502-60-0
Molecular Formula:C12H16O4
Molecular Weight:224.257
Hs Code.:2914509090
DSSTox Substance ID:DTXSID90472878
Wikidata:Q82302066
Mol file:531502-60-0.mol

Synonyms:531502-60-0;1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one;DTXSID90472878;Ethanone, 1-(3-ethyl-2-hydroxy-4,6-dimethoxyphenyl)-;Ethanone,1-(3-ethyl-2-hydroxy-4,6-dimethoxyphenyl)-(9ci)

Suppliers and Price of 1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one

Chemical Property:

PSA：55.76000
LogP:2.17440
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:224.10485899
Heavy Atom Count:16
Complexity:241

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=C(C(=C(C=C1OC)OC)C(=O)C)O

Technology Process of 1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one

There total 5 articles about 1-(3-Ethyl-2-hydroxy-4,6-dimethoxyphenyl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19672-01-6
2-ethyl-3,5-dimethoxyphenol

: 108-24-7
acetic anhydride

: 531502-60-0
1-(3-ethyl-2-hydroxy-4,6-dimethoxy-phenyl)-ethanone

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1002/jhet.5570390620

Reference yield:

: 90-24-4
2-hydroxy-4,6-dimethoxyacetophenone

: 531502-60-0
1-(3-ethyl-2-hydroxy-4,6-dimethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: (C₂H₅)3SiH / trifluoroacetic acid / 20 °C

2: BF₃*Et₂O

With triethylsilane; boron trifluoride diethyl etherate; In trifluoroacetic acid;
DOI:10.1002/jhet.5570390620

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 531502-60-0
1-(3-ethyl-2-hydroxy-4,6-dimethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: BF₃*Et₂O

2: anhydr. K₂CO₃ / acetone / 0.5 h / 50 - 60 °C

3: (C₂H₅)3SiH / trifluoroacetic acid / 20 °C

4: BF₃*Et₂O

With triethylsilane; boron trifluoride diethyl etherate; potassium carbonate; In acetone; trifluoroacetic acid;
DOI:10.1002/jhet.5570390620