1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI)

Base Information

Chemical Name:1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI)
CAS No.:533914-51-1
Molecular Formula:C13H24O2
Molecular Weight:212.33
Hs Code.:
Mol file:533914-51-1.mol

Synonyms:1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI)

Suppliers and Price of 1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI)

There total 2 articles about 1,5-Dioxaspiro[5.5]undecane,8-ethyl-2,4-dimethyl-,(2R,4R,8R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-68-7
cyclohexenone

: 557-20-0
diethylzinc

: 42075-32-1
(2R,4R)-pentanediol

: 533914-51-1
(2R,4R,8R)-8-ethyl-2,4-dimethyl-1,5-dioxaspiro[5.5]undecane

: 533914-51-1
(2R,4R,8S)-8-ethyl-2,4-dimethyl-1,5-dioxaspiro[5.5]undecane

Guidance literature:: cyclohexenone; diethylzinc; With copper(II) bis(trifluoromethanesulfonate); (R)-3,3'-bis[2-(methylthio)ethyl]-1,1'-binaphthalene-2,2'-diol; at 0 ℃; for 2h;

(2R,4R)-pentanediol; With toluene-4-sulfonic acid; orthoformic acid triethyl ester; In benzene; at 20 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(02)00838-8

Reference yield:

: 930-68-7
cyclohexenone

: 557-20-0
diethylzinc

: 42075-32-1
(2R,4R)-pentanediol

: 533914-51-1
(2R,4R,8R)-8-ethyl-2,4-dimethyl-1,5-dioxaspiro[5.5]undecane

: 533914-51-1
(2R,4R,8S)-8-ethyl-2,4-dimethyl-1,5-dioxaspiro[5.5]undecane

Guidance literature:: cyclohexenone; diethylzinc; With copper(II) bis(trifluoromethanesulfonate); (R)-3,3'-bis[2-(methylthio)ethyl]-1,1'-binaphthalene-2,2'-diol; at 0 ℃; for 2h;

(2R,4R)-pentanediol; With toluene-4-sulfonic acid; orthoformic acid triethyl ester; In benzene; at 20 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(02)00838-8