2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone

Base Information

Chemical Name:2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone
CAS No.:59656-68-7
Molecular Formula:C10H11IO4
Molecular Weight:322.099
Hs Code.:

Synonyms:2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone

Suppliers and Price of 2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone

Chemical Property:

Melting Point:201°C
PSA：55.76000
LogP:2.21660

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone

There total 4 articles about 2-Hydroxy-3-iodo-4,6-dimethoxy acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 90-24-4
2-hydroxy-4,6-dimethoxyacetophenone

: 59656-68-7
1-(2-hydroxy-3-iodo-4,6-dimethoxyphenyl)ethan-1-one

Guidance literature:: With hydrogenchloride; potassium iodate; acetic acid; potassium iodide; In water; at 20 ℃; for 4.75h;
DOI:10.1016/j.tetlet.2012.03.079

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 59656-68-7
1-(2-hydroxy-3-iodo-4,6-dimethoxyphenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: I₂, aq. HNO₃, AcOH / acetone

With iodine; nitric acid; potassium carbonate; acetic acid; In acetone;

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 59656-68-7
1-(2-hydroxy-3-iodo-4,6-dimethoxyphenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc(II) chloride; hydrogenchloride / diethyl ether; water / 12 h / 0 - 70 °C

1.2: 2 h

2.1: potassium carbonate / acetone / 2.5 h / Reflux

3.1: iodine; iodic acid / water; ethanol / 2.5 h / 20 °C

With hydrogenchloride; iodine; iodic acid; potassium carbonate; zinc(II) chloride; In diethyl ether; ethanol; water; acetone;