Benzoic acid, 2-amino-, labeled with tritium (9CI)

Base Information

• Chemical Name: Benzoic acid, 2-amino-, labeled with tritium (9CI)
• CAS No.: 50816-84-7
• Molecular Formula: C7H7NO2
• Molecular Weight: 0
• Mol file: 50816-84-7.mol

Synonyms:Benzoic acid, 2-amino-, labeled with tritium (9CI)

Chemical Property of Benzoic acid, 2-amino-, labeled with tritium (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-amino-, labeled with tritium (9CI)

There total 374 articles about Benzoic acid, 2-amino-, labeled with tritium (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

2-nitro-benzaldehyde (552-89-6) → 2-Aminobenzyl alcohol (5344-90-1) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4)

Guidance literature:

With graphitic carbon nitride; hydrazine hydrate; In water; at 90 ℃; for 4h; chemoselective reaction; Irradiation; Sealed tube; Green chemistry;

DOI:10.1002/asia.201800515

Reference yield: 37.0%

o-acetylamino-benzoic acid (89-52-1) → 2-Aminobenzyl alcohol (5344-90-1) + 2-acetamidobenzyl alcohol (20939-77-9) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4)

Guidance literature:

With samarium diiodide; water; In tetrahydrofuran; for 0.0333333h; Ambient temperature;

DOI:10.1246/cl.1993.1495

Reference yield: 27.0%

ortho-nitrobenzoic acid (552-16-9,104810-18-6) → 2-Aminobenzyl alcohol (5344-90-1) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4)

Guidance literature:

With hydrogenchloride; samarium; In methanol; for 0.166667h; Ambient temperature;

DOI:10.1248/cpb.42.402

upstream raw materials:

2-methyl-1H-indole

2-(Benzoylamino)benzoic Acid

phthalic anhydride

phthalimide

Downstream raw materials:

2-((2-hydroxyethyl)amino)benzoic acid

o-carboxysuccinanilic acid

2-Nicotinoylaminobenzoesaeure

4-(2-carboxy-phenylhydrazono)-3-methyl-pentenedioic acid-anhydride

Refernces

• 1、 Buscemi, Silvestre,Insuasty, Braulio,Marzullo, Paola,Moreno, Leydi Marcela,Piccionello, Antonio Palumbo. "Synthesis of oxazolidinones from N-aryl-carbamate and epichlorohydrin under mild conditions". supporting information. p. 140 - 155. Retrieved 2022/03/27.
• 2、 Yao, Hong,Uras, Giuseppe,Zhang, Pengfei,Xu, Shengtao,Yin, Ying,Liu, Jie,Qin, Shuai,Li, Xinuo,Allen, Stephanie,Bai, Renren,Gong, Qi,Zhang, Haiyan,Zhu, Zheying,Xu, Jinyi. "Discovery of Novel Tacrine-Pyrimidone Hybrids as Potent Dual AChE/GSK-3 Inhibitors for the Treatment of Alzheimer's Disease". supporting information. p. 7483 - 7506. Retrieved 2021/06/28.