1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI)

Base Information

Chemical Name:1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI)
CAS No.:585525-11-7
Molecular Formula:C7H8N2O5
Molecular Weight:200.15
Hs Code.:
Mol file:585525-11-7.mol

Synonyms:1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI)

Suppliers and Price of 1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

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Technology Process of 1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI)

There total 1 articles about 1H-Pyrrole-2-carboxylicacid,3-methoxy-1-methyl-4-nitro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 389615-04-7
3-methoxy-1-methyl-4-nitro-1H-pyrrole-2-carboxylic ethyl ester

: 585525-11-7
3-methoxy-1-methyl-4-nitro-1H-pyrrole-2-carboxylic acid

Guidance literature:: With sodium hydroxide; In ethanol; at 20 ℃; for 13h;
DOI:10.1002/chem.200204689

Reference yield: 97.0%

: 36692-49-6
Methyl 3,4-diaminobenzoate

: 585525-11-7
3-methoxy-1-methyl-4-nitro-1H-pyrrole-2-carboxylic acid

: 585525-13-9
4-amino-3-[(3-methoxy-1-methyl-4-nitro-1H-pyrrole-2-carbonyl)-amino]benzoic methyl ester

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.1002/chem.200204689

Reference yield:

: 585525-11-7
3-methoxy-1-methyl-4-nitro-1H-pyrrole-2-carboxylic acid

: 2-(4-amino-3-methoxy-1-methyl-1H-pyrrol-2-yl)-1H-benzoimidazole-5-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / HBTU; Et₃N / dimethylformamide / 20 h / 20 °C

2: 98 percent / AcOH / 12 h / 140 °C

3: TiCl₂*2H₂O / dimethylformamide; acetonitrile / 14 h / 50 °C

With titanium chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.200204689