Sulfamide, (4-bromophenyl)- (9CI)

Base Information

• Chemical Name: Sulfamide, (4-bromophenyl)- (9CI)
• CAS No.: 556068-14-5
• Molecular Formula: C6H7BrN2O2S
• Molecular Weight: 251.10098
• Mol file: 556068-14-5.mol

Synonyms:Sulfamide, (4-bromophenyl)- (9CI)

Chemical Property of Sulfamide, (4-bromophenyl)- (9CI)

Chemical Property:

• PSA: 80.57000
• LogP: 2.91860

Purity/Quality:

95% ^*data from raw suppliers

(4-BROMOPHENYL)SULFAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Sulfamide, (4-bromophenyl)- (9CI)

There total 2 articles about Sulfamide, (4-bromophenyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-bromophenyl)-N'-(tert-butoxycarbonyl)sulfamide (352275-05-9) → C6H7BrN2O2S (556068-14-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1016/S0960-894X(03)00028-3

Reference yield:

4-bromo-aniline (106-40-1) → C6H7BrN2O2S (556068-14-5)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 0 °C

2: TFA / CH₂Cl₂

With triethylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1016/S0960-894X(03)00028-3

Reference yield: 87.0%

2-chloro-6-methylquinoline-3-carbaldehyde (73568-27-1) + C6H7BrN2O2S (556068-14-5) + triethyl phosphite (122-52-1) → C21H24BrClN3O5PS

Guidance literature:

In neat (no solvent); for 0.233333h; Ionic liquid; Sonication; Green chemistry;

DOI:10.1002/ardp.202000291

upstream raw materials:

N-(4-bromophenyl)-N'-(tert-butoxycarbonyl)sulfamide

4-bromo-aniline

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