2，6-dimethyl phenyl hydrazine

Base Information

• Chemical Name: 2，6-dimethyl phenyl hydrazine
• CAS No.: 603-77-0
• Molecular Formula: C8H12N2
• Molecular Weight: 136.197
• Hs Code.: 2928000090
• Mol file: 603-77-0.mol

Synonyms:(2,6-DIMETHYL-PHENYL)-HYDRAZINE

Chemical Property of 2，6-dimethyl phenyl hydrazine

Chemical Property:

• PSA: 38.05000
• LogP: 2.36230

Purity/Quality:

98%min ^*data from raw suppliers

(2,6-dimethylphenyl)hydrazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2，6-dimethyl phenyl hydrazine

There total 4 articles about 2，6-dimethyl phenyl hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,6-dimethylaniline (87-62-7) → (2,6-dimethylphenyl)hydrazine (603-77-0)

Guidance literature:

2,6-dimethylaniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃; for 0.333333h;

With hydrogenchloride; tin(ll) chloride; In water; at 0 - 20 ℃; for 6.08333h;

Reference yield:

→ (2,6-dimethylphenyl)hydrazine (603-77-0)

Guidance literature:

With tin(ll) chloride;

DOI:10.1021/ja01526a057

Reference yield:

2,6-Dimethylphenyl diazonium chloride (85518-80-5) → (2,6-dimethylphenyl)hydrazine (603-77-0)

Guidance literature:

With tin(ll) chloride;

upstream raw materials:

2,6-dimethylaniline

2,6-Dimethylphenyl diazonium chloride

Downstream raw materials:

benzyl-3-(2,6-dimethylphenyl)dithiocarbazate

N-(2,6-dimethylphenyl)-N'-ethoxycarbonylhydrazine

2-methylindole-3-carboxaldehyde 2,6-dimethylphenylhydrazone

Mesitylencarbonsaeure-(2,6-dimethyl-phenylhydrazid)

Refernces

• 1、 Nagarajan, K.,Talwalker, P.K.,Kulkarni, C.L.,Venkateswarlu, A.,Prabhu, S.S.,Nayak, G.V.. "Antiimplantation Agents: Part I - 1-Arylthiosemicarbazides". . p. 1243 - 1257. Retrieved 2007/10/02.