1,2,5-Oxadiazole-3-carbonyl chloride, 4-methyl- (9CI)

Base Information

• Chemical Name: 1,2,5-Oxadiazole-3-carbonyl chloride, 4-methyl- (9CI)
• CAS No.: 15323-68-9
• Molecular Formula: C4H3 Cl N2 O2
• Molecular Weight: 146.53182
• Hs Code.: 2934999090
• Mol file: 15323-68-9.mol

Synonyms:Furazancarbonylchloride, methyl- (8CI); 4-Methyl-1,2,5-oxadiazole-3-carbonyl chloride

Chemical Property of 1,2,5-Oxadiazole-3-carbonyl chloride, 4-methyl- (9CI)

Chemical Property:

• PSA: 55.99000
• LogP: 0.75700

Purity/Quality:

98%min ^*data from raw suppliers

4-Methyl-1,2,5-oxadiazole-3-carbonylchloride 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,5-Oxadiazole-3-carbonyl chloride, 4-methyl- (9CI)

There total 2 articles about 1,2,5-Oxadiazole-3-carbonyl chloride, 4-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-1,2,5-oxadiazole-3-carboxylic acid (58677-34-2) → 4-methyl-1,2,5-oxadiazole-3-carbonyl chloride (15323-68-9)

Guidance literature:

With thionyl chloride; at 80 ℃; for 2h;

Reference yield:

→ 4-methyl-1,2,5-oxadiazole-3-carbonyl chloride (15323-68-9)

Guidance literature:

3-Methyl-4-furazancarbonsaeure, SOCl2/DMF;

Reference yield:

4-methyl-1,2,5-oxadiazole-3-carbonyl chloride (15323-68-9) + N-((R)-(2-((S)-amino(4,4-difluorocyclohexyl)methyl)imidazo[1,2-α]pyrimidin-7-yl)(cyclopropyl)methyl)-2-(3,3-difluorocyclobutyl)acetamide → N-((S)-(7-((R)-cyclopropyl(2-(3,3-difluorocyclobutyl)acetamido)methyl)imidazo[1,2-α]pyrimidin-2-yl)(4,4-difluorocyclohexyl)methyl)-4-methyl-1,2,5-oxadiazole-3-carboxamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 19.75h;

upstream raw materials:

4-methyl-1,2,5-oxadiazole-3-carboxylic acid

Downstream raw materials:

3-Amino-4-pyrrolidino-carbonylfurazan

3-Methyl-4-morpholino-carbonylfurazan

4-Methylfurazan-3-N-isopropylcarboxamid

4-Methylfurazan-3-N-methylcarboxamid

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