N-[(E)-2-Furylmethylidene]-2-phenylethanamine

Base Information

• Chemical Name: N-[(E)-2-Furylmethylidene]-2-phenylethanamine
• CAS No.: 69819-53-0
• Molecular Formula: C13H13NO
• Molecular Weight: 199.252
• Mol file: 69819-53-0.mol

Synonyms:N-[(E)-2-Furylmethylidene]-2-phenylethanamine

Chemical Property of N-[(E)-2-Furylmethylidene]-2-phenylethanamine

Chemical Property:

• PSA: 25.50000
• LogP: 2.94120

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-[(E)-2-Furylmethylidene]-2-phenylethanamine

There total 2 articles about N-[(E)-2-Furylmethylidene]-2-phenylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

furfural (98-01-1) + phenethylamine (64-04-0) → N-(2-furylmethylidene)-2-phenylethylamine (69819-53-0)

Guidance literature:

In diethyl ether; Molecular sieve; Inert atmosphere;

DOI:10.1002/cbic.202000503

Reference yield: 85.0%

furfural (98-01-1) + phenethylamine (64-04-0) → furfural-phenethylimine (69819-53-0)

Guidance literature:

With 4 A molecular sieve; In diethyl ether; Ambient temperature;

DOI:10.1021/jo00116a027

Reference yield: 98.0%

methyl magnesium iodide (917-64-6) + furfural-phenethylimine (69819-53-0) → (1-Furan-2-yl-ethyl)-phenethyl-amine

Guidance literature:

With 1-(trimethylsilyl)-1H-benzotriazole; In diethyl ether; toluene; for 20h; Heating;

DOI:10.1021/jo00116a027

upstream raw materials:

furfural

phenethylamine

Downstream raw materials:

N-(furan-2-ylmethyl)-2-phenylethan-1-amine

4-oxo-3-phenethyl-10-oxa-3-azatricyclo[5.2.1.0^1,5]dec-8-ene-6-carboxylic acid

3-oxo-2-phenethyl-2,3-dihydro-1H-isoindole-5-carboxylic acid

bis(N-furfuryl-N-(2-phenylethyl)dithiocarbamato-S,S')lead(II)

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