N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide

Base Information

Chemical Name:N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide
CAS No.:60166-97-4
Molecular Formula:C14H19N3O8
Molecular Weight:357.32
Hs Code.:
DSSTox Substance ID:DTXSID60701001
Wikidata:Q82632558
Mol file:60166-97-4.mol

Synonyms:60166-97-4;DTXSID60701001;N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide

Suppliers and Price of N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide

Chemical Property:

Boiling Point:774.2±60.0 °C(Predicted)
PKA:11.85±0.46(Predicted)
PSA：191.13000
Density:1.496±0.06 g/cm3(Predicted)
LogP:-0.75030
XLogP3:-2.5
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:8
Exact Mass:357.11721457
Heavy Atom Count:25
Complexity:463

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C=C1C(=O)N(C(CO)CO)C(CO)CO)[N+](=O)[O-])C(=O)N

Technology Process of N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide

There total 1 articles about N~1~,N~1~-Bis(1,3-dihydroxypropan-2-yl)-5-nitrobenzene-1,3-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 13290-96-5
dimethyl 5-nitroisophthalate

: 534-03-2
serinol

: 60166-97-4
N,N'-bis-(2-hydroxy-1-hydroxymethylethyl)-5-nitroisophthalamide

Guidance literature:: In methanol; at 20 ℃; for 48h; Reflux;

Reference yield:

: 60166-97-4
N,N'-bis-(2-hydroxy-1-hydroxymethylethyl)-5-nitroisophthalamide

: 267881-76-5
5-amino-N,N'-bis[2-hydroxy-1-(hydroxymethyl)ethyl]-1,3-benzenedicarboxamide

Guidance literature:: With hydrogen; In water; for 10h; under 11251.1 Torr;

Reference yield:

: 60166-97-4
N,N'-bis-(2-hydroxy-1-hydroxymethylethyl)-5-nitroisophthalamide

: 60166-98-5
S-N,N'-bis[2-hydroxy-1-(hydroxymethyl)ethyl]-5-amino-2,4,6-triiodo-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / water / 10 h / 11251.1 Torr

2: iodine; potassium iodate; sodium sulfate; sulfuric acid / water / 47 h / 65 - 80 °C

With potassium iodate; sulfuric acid; hydrogen; iodine; sodium sulfate; In water;