5-P-tolyloxy-furan-2-carbaldehyde

Base Information

• Chemical Name: 5-P-tolyloxy-furan-2-carbaldehyde
• CAS No.: 60698-29-5
• Molecular Formula: C12H10O3
• Molecular Weight: 202.21
• Hs Code.: 2932190090
• DSSTox Substance ID: DTXSID20514992
• Wikidata: Q82375631
• Mol file: 60698-29-5.mol

Synonyms:5-P-tolyloxy-furan-2-carbaldehyde;60698-29-5;5-(p-Tolyloxy)furan-2-carbaldehyde;5-(p-tolyloxy)furfural;5-(4-METHYLPHENOXY)FURAN-2-CARBALDEHYDE;DTXSID20514992;FT-0692622

Chemical Property of 5-P-tolyloxy-furan-2-carbaldehyde

Chemical Property:

• PSA: 39.44000
• LogP: 3.19280
• XLogP3: 3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 202.062994177
• Heavy Atom Count: 15
• Complexity: 209

Purity/Quality:

97% ^*data from raw suppliers

5-PARA-TOLYLOXY-FURAN-2-CARBALDEHYDE 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)OC2=CC=C(O2)C=O

Technology Process of 5-P-tolyloxy-furan-2-carbaldehyde

There total 2 articles about 5-P-tolyloxy-furan-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-2-furancarboxaldehyde (1899-24-7) + p-cresol (106-44-5) → 5-(4-methylphenoxy)-2-furancarboxaldehyde (60698-29-5)

Guidance literature:

With sodium; Yield given. Multistep reaction; 1) DMSO; 2) 4 h, steam bath;

Reference yield:

→ 5-(4-methylphenoxy)-2-furancarboxaldehyde (60698-29-5)

Guidance literature:

2-p-Tolyloxy-furan IVa, DMF, POCl3;

DOI:10.1007/BF00757689

Reference yield: 87.5%

5-(4-methylphenoxy)-2-furancarboxaldehyde (60698-29-5) + malononitrile (109-77-3) → 2-(5-p-Tolyloxy-furan-2-ylmethylene)-malononitrile (78427-15-3)

Guidance literature:

With sodium ethanolate; In ethanol; for 3h; Ambient temperature;

upstream raw materials:

5-bromo-2-furancarboxaldehyde

p-cresol

Downstream raw materials:

5-p-tolyloxy-furan-2-carboxylic acid

5-(4-methylphenoxy)-2-furonitrile

2-(5-p-Tolyloxy-furan-2-ylmethylene)-malononitrile

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