BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE

Base Information

• Chemical Name: BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE
• CAS No.: 703-06-0
• Molecular Formula: C8H10FO2P
• Molecular Weight: 188.138
• Mol file: 703-06-0.mol

Synonyms:BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE;Benzenephosphonic acid ethyl ester fluoride 97%;Benzenephosphonicacidethylesterfluoride97%;BENZENEPHOSPHONIC ACID ETHYL ESTER FLUOROIDE

Chemical Property of BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE

Chemical Property:

• Vapor Pressure: 0.0405mmHg at 25°C
• Refractive Index: 1.467
• Boiling Point: 95°C 2mm
• Flash Point: 103.4°C
• PSA: 36.11000
• Density: 1,188 g/cm3
• LogP: 2.51100

Purity/Quality:

98%Min ^*data from raw suppliers

BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE

There total 8 articles about BENZENEPHOSPHONIC ACID ETHYL ESTER FLUORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

EPN oxon (2012-00-2,68887-74-1,68887-75-2) → (ethoxy)phenylfluorophosphinate (703-06-0)

Guidance literature:

With fluoride on polymer; In acetonitrile; at 20 ℃;

DOI:10.1002/cbic.202000852

Reference yield: 36.0%

ethyl hydrogen phenylphosphonate (4546-19-4) → (ethoxy)phenylfluorophosphinate (703-06-0)

Guidance literature:

With sodium fluoride; trifluoroacetic anhydride; In dimethyl sulfoxide; acetonitrile; at 100 ℃; for 11h; Inert atmosphere;

Reference yield: 30.0%

ethyl Phenylphosphinate (172487-18-2,2511-09-3) → (ethoxy)phenylfluorophosphinate (703-06-0)

Guidance literature:

With sodium fluoride; trifluoroacetic anhydride; In dimethyl sulfoxide; acetonitrile; at 100 ℃; for 11h; Inert atmosphere;

upstream raw materials:

ethanol

Phenylphosphoroxid-fluoridchlorid

ethyl trimethylsilyl ether

phenyltetrafluorophosphorane

Downstream raw materials:

C₁₇H₂₁N₂O₃P

O-(O-Aethyl-phenyl-phosphonyl)-N,N-dimethylbenzamidoxim

Refernces

• 1、 -. "Preparation method of phosphoryl fluoride compound". Paragraph 0139-0142. . Retrieved 2021/11/03.