3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI)

Base Information

Chemical Name:3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI)
CAS No.:677762-00-4
Molecular Formula:C8H9NO3
Molecular Weight:167.164
Hs Code.:
Mol file:677762-00-4.mol

Synonyms:3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI)

Suppliers and Price of 3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-Ethyl-6-oxo-1,6-dihydropyridine-3-carboxylicacid 97%
1g
$ 513.00

A1 Biochem Labs
1-Ethyl-6-oxo-1,6-dihydropyridine-3-carboxylicacid 95%
5 g
$ 1050.00

Total 3 raw suppliers

Chemical Property of 3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI)

Chemical Property:

PSA：59.30000
LogP:0.56640

Purity/Quality:

97% ^*data from raw suppliers

1-Ethyl-6-oxo-1,6-dihydropyridine-3-carboxylicacid 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI)

There total 6 articles about 3-Pyridinecarboxylicacid,1-ethyl-1,6-dihydro-6-oxo-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.2%

: 74925-38-5
methyl 1-ethyl-6-oxo-1,6-dihydropyridine-3-carboxylate

: 677762-00-4
1-ethyl-2-pyridone-5-carboxylic acid

Guidance literature:: methyl 1-ethyl-6-oxo-1,6-dihydropyridine-3-carboxylate; With lithium hydroxide; water; In 1,4-dioxane; for 2h;

Product distribution / selectivity; Acidic aqueous solution;

Reference yield: 89.0%

: benzyl 1-ethyl-6-oxo-1,6-dihydropyridine-3-carboxylate

: 677762-00-4
1-ethyl-2-pyridone-5-carboxylic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 2h;

Reference yield:

: 66171-50-4
methyl 6-hydroxynicotinate

: 677762-00-4
1-ethyl-2-pyridone-5-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 16 h / 80 °C

2: water; lithium hydroxide monohydrate / tetrahydrofuran / 2 h / 20 °C

With lithium hydroxide monohydrate; water; potassium carbonate; In tetrahydrofuran; acetonitrile;