5-TERT-BUTYL-2-CHLORO-3-HYDROXYMETHYLENE-CYCLOHEX-1-ENE CARBOXALDEHYDE

Base Information

• Chemical Name: 5-TERT-BUTYL-2-CHLORO-3-HYDROXYMETHYLENE-CYCLOHEX-1-ENE CARBOXALDEHYDE
• CAS No.: 61009-99-2
• Molecular Formula: C12H17ClO2
• Molecular Weight: 228.719
• Hs Code.: 2913000090
• Mol file: 61009-99-2.mol

Synonyms:5-TERT-BUTYL-2-CHLORO-3-HYDROXYMETHYLENE-CYCLOHEX-1-ENE CARBOXALDEHYDE

Chemical Property of 5-TERT-BUTYL-2-CHLORO-3-HYDROXYMETHYLENE-CYCLOHEX-1-ENE CARBOXALDEHYDE

Chemical Property:

• PSA: 37.30000
• LogP: 3.57620

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-TERT-BUTYL-2-CHLORO-3-HYDROXYMETHYLENE-CYCLOHEX-1-ENE CARBOXALDEHYDE

There total 2 articles about 5-TERT-BUTYL-2-CHLORO-3-HYDROXYMETHYLENE-CYCLOHEX-1-ENE CARBOXALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-tercbutyl-cyclohexanone (98-53-3) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 5-(tert-butyl)-2-chloro-3-(hydroxymethylene)cyclohex-1-ene-1-carbaldehyde (61009-99-2)

Guidance literature:

N,N-dimethyl-formamide; With trichlorophosphate; In dichloromethane; at 0 ℃; for 0.5h;

4-tercbutyl-cyclohexanone; In dichloromethane; at 80 ℃; for 3h;

DOI:10.3762/bjoc.17.133

Reference yield:

→ 5-(tert-butyl)-2-chloro-3-(hydroxymethylene)cyclohex-1-ene-1-carbaldehyde (61009-99-2)

Guidance literature:

4-tert-Butylcyclohexanon, DMF, POCl3;

DOI:10.1021/jo00425a027

Reference yield: 86.0%

5-(tert-butyl)-2-chloro-3-(hydroxymethylene)cyclohex-1-ene-1-carbaldehyde (61009-99-2) + aniline hydrochloride (142-04-1,36663-09-9) → N-[(3-(anilinomethylene)-2-chloro-5-tert-butyl-1-cyclohexen-1-yl)methylene]aniline hydrochloride (731863-07-3)

Guidance literature:

In methanol; chloroform; for 3.33333h; Heating;

DOI:10.1021/jacs.6b06361

upstream raw materials:

4-tercbutyl-cyclohexanone

N,N-dimethyl-formamide

Downstream raw materials:

C₄₁H₄₁ClN₄O

6-((E)-2-((E)-2-(5-tert-butyl-2-chloro-3-((E)-2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)cyclohex-2-enylidene)ethylidene)-3,3-dimethylindolin-1-yl)hexanoic acid

2-(4-((E)-2-((E)-3-((E)-2-(1-(4-bromobenzyl)-3,3-dimethylindolin-2-ylidene)ethylidene)-5-tert-butyl-2-chlorocyclohex-1-enyl)vinyl)-3-cyano-5,5-dimethylfuran-2(5H)-ylidene)malononitrile

2-(4-((E)-2-((E)-3-((E)-2-(1-benzyl-3,3-dimethylindolin-2-ylidene)ethylidene)-5-tert-butyl-2-(phenoxy)cyclohex-1-enyl)vinyl)-3-cyano-5,5-dimethylfuran-2(5H)-ylidene)malononitrile

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