Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI)

Base Information

Chemical Name:Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI)
CAS No.:688359-69-5
Molecular Formula:C11H16O3
Molecular Weight:196.246
Hs Code.:
Mol file:688359-69-5.mol

Synonyms:Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI)

Suppliers and Price of Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI)

Chemical Property:

PSA：30.99000
LogP:1.31850

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI)

There total 1 articles about Dispiro[1,3-dioxolane-2,1(4H)-pentalene-4,2-oxirane], hexahydro-, (2R,3aS,6aS)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3084-53-5
trimethylsulphonium bromide

: hexahydro-4’H-spiro[1,3-dioxolane-2,1’-pentalen]-4’-one

: 688359-69-5
C₁₁H₁₆O₃

Guidance literature:: With potassium hydroxide; In water; acetonitrile; at 60 ℃;
DOI:10.1016/j.tetasy.2003.11.040

Reference yield: 89.0%

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 688359-69-5
C₁₁H₁₆O₃

: 688359-70-8
(1S,5S,6S,1'R)-6-hydroxy-6-(1-phenylethyl-aminomethyl)-bicyclo[3.3.0]octan-2-one ethylene ketal

Guidance literature:: In ethanol; Heating;
DOI:10.1016/j.tetasy.2003.11.040

Reference yield:

: 688359-69-5
C₁₁H₁₆O₃

: (1S,5S,6S,1'R)-6-hydroxy-6-(1-phenylethyl-aminomethyl)-bicyclo[3.3.0]octan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / ethanol / Heating

2: 100 percent / HCl / acetone / 5 h / 20 °C

With hydrogenchloride; In ethanol; acetone;
DOI:10.1016/j.tetasy.2003.11.040